Chains of fused rings in the hydrogen-bonded structure of meso-6,13-diamino-6,13-dimethyl-1,4,8,11-tetraazacyclotetradecane-2,2′-biphenol (1/2)

被引：2

作者：

Lough, AJ

Gregson, RM

Ferguson, G

Glidewell, C ^{[1
]}

机构：

[1] Univ St Andrews, Sch Chem, St Andrews KY16 9ST, Fife, Scotland

[2] Univ Toronto, Lash Miller Chem Labs, Toronto, ON M5S 3H6, Canada

[3] Univ Guelph, Dept Chem & Biochem, Guelph, ON N1G 2W1, Canada

来源：

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 2000年 / 56卷 / 07期

关键词：

D O I：

10.1107/S0108270100005527

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The title compound is a salt, [C12H32N6](2+). 2[HOC6H4C6H4O](-). The centrosymmetric cation contains two intramolecular ND H ... N hydrogen bonds with an N ... N distance of 2.8290 (13) Angstrom, and the pendent amino groups are in axial sites; the anion contains an intramolecular O-H ... O hydrogen bond with an O ... O distance of 2.4656 (11) Angstrom. The ions are linked into continuous chains by means of four types of N-H ... O hydrogen bonds with N ... O distances ranging from 2.7238 (12) Angstrom to 3.3091 (13) Angstrom, associated with N-H ... O angles in the range 148-160 degrees.

引用

页码：859 / 861

页数：3

共 12 条

[1] ADAM KR, 1994, CHEM COMMUN, P1539
[2] THERMODYNAMIC AND STRUCTURAL STUDIES OF CONFIGURATIONAL ISOMERS OF [NI(CYCLAM)]2+
BAREFIELD, EK
BIANCHI, A
BILLO, EJ
CONNOLLY, PJ
PAOLETTI, P
SUMMERS, JS
VANDERVEER, DG
[J]. INORGANIC CHEMISTRY, 1986, 25 (23) : 4197 - 4202
[3] Crystal engineering using bis- and tris-phenols.: Adducts with 1,4,8,11-tetraazacyclotetradecane (cyclam):: Isolated ladders in the adduct with 4,4′-thiodiphenol, tethered ladders in the adduct with 4,4′-sulfonyldiphenol and two interwoven three-dimensional networks in the adduct with 1,1,1-tris(4-hydroxyphenyl)ethane
Ferguson, G
Glidewell, C
Gregson, RM
Meehan, PR
[J]. ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 1998, 54 : 139 - 150
[4] A chain of fused R22(10) and R46(12) rings in the hydrogen-bonded structure of 1,4,8,11-tetraazacyclotetradecane-2,2′-biphenol (1/2)
Ferguson, G
Gregson, RM
Glidewell, C
[J]. ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1999, 55 : 815 - 817
[5] FERGUSON G, 1999, PRPKAPPA
[6] meso-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane as a building block in supramolecular chemistry;: salts formed with 2,2′-biphenol, 4,4′-biphenol, 4,4′-thiodiphenol, 4,4′-sulfonyldiphenol, 3- and 4-hydroxybenzoic acids, 3,5-dihydroxybenzoic acid and phenylphosphonic acid;: supramolecular structures in zero, one, two and three dimensions
Gregson, RM
Glidewell, C
Ferguson, G
Lough, AJ
[J]. ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE CRYSTAL ENGINEERING AND MATERIALS, 2000, 56 (56): : 39 - 57
[7] Johnson C. K., 1976, ORNL5138
[8] Two different three-dimensional hydrogen-bonded framework structures in two hydrated adducts meso-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-terephthalic acid-water (1/1/4) and (1/1/6)
Lough, AJ
Gregson, RM
Ferguson, G
Glidewell, C
[J]. ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE CRYSTAL ENGINEERING AND MATERIALS, 2000, 56 (56) : 85 - 93
[9] *NON BV, 1997, KAPPACCD SERV SOFTW
[10] Processing of X-ray diffraction data collected in oscillation mode
Otwinowski, Z
Minor, W
[J]. MACROMOLECULAR CRYSTALLOGRAPHY, PT A, 1997, 276 : 307 - 326

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