One-pot hydrothermal synthesis of uniformly cubic Co3O4 nanocrystals

被引：50

作者：

Teng, Yonghong ^{[1
]}

Yamamoto, Shinpei ^{[2
]}

Kusano, Yoshihiro ^{[3
]}

Azuma, Masaki ^{[1
]}

Shimakawa, Yuichi ^{[1
]}

机构：

[1] Kyoto Univ, Inst Chem Res, Uji, Kyoto 6110011, Japan

[2] Kyoto Univ, Inst Integrated Cell Mat Sci, Sakyo Ku, Kyoto 6068501, Japan

[3] Kurashiki Univ Sci & Arts, Coll Arts, Kurashiki, Okayama 7128505, Japan

来源：

MATERIALS LETTERS | 2010年 / 64卷 / 03期

关键词：

Cubic nanocrystal; Cobalt oxide; Oxidant; Capping reagent; Polyvinylpyrrolidone; Removal; NANOPARTICLES; GENERATION; SOLUBILITY; NANOCUBES;

D O I：

10.1016/j.matlet.2009.10.039

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Cubic Co3O4 nanocrystals (NCs) were synthesized by a one-pot hydrothermal reaction in the presence of the oxidant KClO3 and the capping reagent polyvinylpyrrolidone (PVP). The as-prepared Co3O4 NCs were uniformly cubic with sharp edges and good crystallinity and showed flat surfaces with (100) facets. The capped PVP could be removed without losing cubic shape by heating the NCs at 300 degrees C. (C) 2009 Elsevier B.V. All rights reserved.

引用

页码：239 / 242

页数：4

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