A New 3D Supramolecular Network Formed by [Zn3(2,6-Pyridinedicarboxylate)3Cl4]4- and 4-Carboxypyridinium

被引：0
|
作者：
Yang E [1 ,2 ]
Kang Yao [3 ]
Wang Xiao-Qin [3 ]
Liu Zi-Sheng [2 ]
Li Jun-Qian [1 ,3 ]
机构：
[1] Fuzhou Univ, Dept Chem, Fuzhou 350002, Peoples R China
[2] Fujian Normal Univ, Fujian Key Lab Polymer Mat, Coll Chem & Mat Sci, Fuzhou 350007, Peoples R China
[3] Chinese Acad Sci, Fujian Inst Res Struct Matter, Fuzhou 350002, Fujian, Peoples R China
来源：
CHINESE JOURNAL OF STRUCTURAL CHEMISTRY | 2010年 / 29卷 / 05期
关键词：
crystal structure; 3D supramolecular network; hydrogen bonding array; CRYSTAL;
D O I：
暂无
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
A new compound [Zn-3(C7NO4H3)(3)Cl-4]center dot[C6NO2H6](4)center dot 4H(2)O (I) has been synthesized and structurally characterized by X-ray crystallography. It crystallizes in monoclinic, space group C2/c with a = 16.9018(14), b = 12.6902(10), c = 25.1170(2) angstrom, beta = 90.54 degrees, V = 5387.0(8) angstrom(3), Z = 4, Zn3C45H41Cl4N7O24, M-r = 1401.76, D-c = 1.728 g/cm(3), F(000) = 2840, mu(MoK alpha) = 1.615 mm(-1), the R = 0.0758 and wR = 0.2060 for 3468 observed reflections (I > 20(I)). Analysis of single-crystal X-ray diffraction data shows that compound I displays an interesting example of 3D supramolecular networks with perfect neutral and ionic hydrogen bonding array.
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收藏
页码：774 / 778
页数：5
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