Real surface determination of Co3O4 by Zn2+ adsorption.: A comparison between X-ray diffraction, cyclic voltammetry and adsorption methods

被引：8

作者：

Nkeng, P

Marlier, S

Koenig, JF

Chartier, P

Poillerat, G

Gautier, JL

机构：

[1] Univ Strasbourg 1, Fac Chim, URA CNRS 405, Lab Electrochim & Chim Phys Corps Solide, F-67000 Strasbourg, France

[2] Univ Santiago Chile, Fac Quim & Biol, Lab Electroquim, Santiago 2, Chile

来源：

ELECTROCHIMICA ACTA | 1998年 / 43卷 / 08期

关键词：

real surface area; spinels; metallic oxide;

D O I：

10.1016/S0013-4686(97)00219-3

中图分类号：

O646 [电化学、电解、磁化学];

学科分类号：

081704 ;

摘要：

The real surface areas of Co3O4 films have been measured by Zn2+ adsorption. Co3O4 films have been prepared by spray pyrolysis. The results are compared with crystallite sizes obtained by X-ray diffraction measurements and roughness factors calculated from cyclic voltammograms. Discrepancies between the three methods are discussed and examined. (C) 1997 Elsevier Science Ltd. All rights reserved.

引用

页码：893 / 898

页数：6