Solvothermal synthesis of In(OH)3 nanorods and their conversion to In2O3

被引：15

作者：

Yang, Hongxiao ^{[1
]}

Yang, Zhijie ^{[1
]}

Liang, Hui ^{[1
]}

Liu, Ling ^{[1
]}

Guo, Jinxin ^{[1
]}

Yang, Yanzhao ^{[1
]}

机构：

[1] Shandong Univ, Sch Chem & Chem Engn, Jinan 250100, Shandong, Peoples R China

来源：

MATERIALS LETTERS | 2010年 / 64卷 / 13期

关键词：

Nanomaterials; Solvothermal; In2O3; Nanorods; SENSING PROPERTIES; HYDROTHERMAL SYNTHESIS; NANOCRYSTALS; INDIUM; NANOWIRES; NANOTUBES; GAS; SEMICONDUCTOR; NANOPARTICLES; SENSORS;

D O I：

10.1016/j.matlet.2010.03.030

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

In this work, we demonstrate that monodisperse indium hydroxide (In(OH)(3)) nanorods constructed with parallel wire-like subunits have been fabricated via a acrylamide-assisted synthesis route without any template NH3 from the hydrolysis of acrylamide acts as the OH- provider The structure and morphology of as-prepared products have been characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), high-resolution transmission electron microscopy (HRTEM) and thermogravimetric analysis (TG) A detailed mechanism has been proposed on the basis of time-dependent experimental results Furthermore, by annealing In(OH)(3) precursors at 500 degrees C for 3 h in air, In2O3 samples were obtained with the designed morphology. (C) 2010 Elsevier BV All rights reserved

引用

页码：1418 / 1420

页数：3

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