Nano-hydroxyapatite preparation from biogenic raw materials

被引:47
作者
Gergely, Greta [1 ]
Weber, Ferenc [1 ]
Lukacs, Istvan [1 ]
Illes, Levente [1 ]
Toth, Attila L. [1 ]
Horvath, Zsolt E. [2 ]
Mihaly, Judit [3 ]
Balazsi, Csaba [1 ]
机构
[1] Hungarian Acad Sci, Res Inst Tech Phys & Mat Sci, Ceram & Nanocomposites Dept, H-1121 Budapest, Hungary
[2] Hungarian Acad Sci, Res Inst Tech Phys & Mat Sci, Nanostruct Dept, H-1121 Budapest, Hungary
[3] Hungarian Acad Sci, Chem Res Ctr, IR & Raman Spect Lab, H-1025 Budapest, Hungary
来源
CENTRAL EUROPEAN JOURNAL OF CHEMISTRY | 2010年 / 8卷 / 02期
关键词
HAp; Raw material; Ball milling; Attrition; Characterization; PHOSPHATE; BIOCERAMICS; SPECTROSCOPY; RATIOS; CORAL;
D O I
10.2478/s11532-010-0004-4
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Hydroxyapatite (HAp) was successfully produced from recycled eggshell, seashell and phosphoric acid. The phases obtained depended on the ratio of calcined eggshell/seashell to phosphoric acid, the calcination temperature and the mechanochemical activation method (ball milling or attrition milling). The HAp structures were characterized by X-ray diffraction, scanning electron microsopy and infrared spectroscopy. Attrition milling was more effective than ball milling, yielding nanosize, homogenous and pure Hap.
引用
收藏
页码:375 / 381
页数:7
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