Nanoparticles of the superconductor MgB2:: structural characterization and in situ study of synthesis kinetics

被引：19

作者：

Cui, CX

Liu, DB

Shen, YT

Sun, JB

Meng, FB

Wang, R

Liu, SJ

Greer, AL

Chen, SK

Glowacki, BA

机构：

[1] Hebei Univ Technol, Sch Mat Sci & Engn, Tianjin 300130, Peoples R China

[2] Univ Cambridge, Dept Mat Sci & Met, Cambridge CB2 3QZ, England

来源：

ACTA MATERIALIA | 2004年 / 52卷 / 20期

基金：

中国国家自然科学基金;

关键词：

crystal growth; HREM observation; nanometer particles; reaction kinetics; reaction synthesis;

D O I：

10.1016/j.actamat.2004.08.033

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Single-crystal MgB2 nanoparticles, with diameters in the range 20-100 nm, have been synthesized in situ in the sample chamber of an X-ray diffractometer. The reaction kinetics are analyzed and related to the atomic-level structure of the particles as observed by high-resolution electron microscopy. Synthesis conditions may have a significant influence on microstructure and superconducting properties. (C) 2004 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.

引用

页码：5757 / 5760

页数：4

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