High Field Solid-State NMR Spectroscopy Investigation of 15N-Labeled Rosette Nanotubes: Hydrogen Bond Network and Channel-Bound Water

被引：22

作者：

Fenniri, Hicham ^{[1
,2
,3
]}

Tikhomirov, Grigory A. ^{[2
,3
,5
]}

Brouwer, Darren H. ^{[4
]}

Bouatra, Souhaila ^{[2
,3
,7
]}

El Bakkari, Mounir ^{[2
,3
]}

Yan, Zhimin ^{[3
]}

Cho, Jae-Young ^{[3
]}

Yamazaki, Takeshi ^{[3
,6
]}

机构：

[1] Northeastern Univ, Snell Engn Ctr 313, 360 Huntington Ave, Boston, MA 02115 USA

[2] Univ Alberta, Dept Chem, 11421 Saskatchewan Dr, Edmonton, AB T6G 2M9, Canada

[3] Univ Alberta, Natl Inst Nanotechnol NINT NRC, 11421 Saskatchewan Dr, Edmonton, AB T6G 2M9, Canada

[4] Redeemer Univ Coll, Dept Chem, 777 Garner Rd East, Ancaster, ON L9K 1J4, Canada

[5] CALTECH, Div Biol & Biol Engn, 1200 East Calif Blvd, Pasadena, CA 91125 USA

[6] Vancouver Prostate Ctr, 2660 Oak St, Vancouver, BC V6H 3Z6, Canada

[7] Univ Alberta, Dept Biol Sci, Edmonton, AB 26G 2E8, Canada

来源：

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY | 2016年 / 138卷 / 19期

基金：

加拿大自然科学与工程研究理事会; 加拿大创新基金会;

关键词：

STRUCTURAL DNA NANOTECHNOLOGY; CHEMICAL-SHIFTS; MAS NMR; NANOPARTICLES; MOLECULES; IDENTIFICATION; COMPLEXES; COUPLINGS; LIGANDS; H-1-NMR;

D O I：

10.1021/jacs.6b02420

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

N-15-labeled rosette nanotubes were synthesized and investigated using high-field solid-state NMR spectroscopy, X-ray diffraction, atomic force microscopy, and electron microscopy. The results established the H-bond network involved in the self-assembly of the nanostructure as well as bound water molecules in the nanotube's channel.

引用

页码：6115 / 6118

页数：4

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