Synthesis and X-ray structures of metallocenium diamines of iron and cobalt

被引：11
|
作者：
Inyushin, S
Shafir, A
Sheats, JE
Minihane, M
Whitten, CE
Arnold, J [1 ]
机构：
[1] Rider Univ, Dept Chem, Lawrenceville, NJ 08648 USA
[2] Univ Calif Berkeley, Lawrence Berkeley Lab, Div Chem Sci, Berkeley, CA 94720 USA
[3] Bowdoin Coll, Dept Chem, Brunswick, ME 04011 USA
[4] Univ Calif Berkeley, Dept Chem, Berkeley, CA 94720 USA
来源：
POLYHEDRON | 2004年 / 23卷 / 17期
关键词：
metallocene; ferrocenium; cobaltocenium; crystal structure;
D O I：
10.1016/j.poly.2004.08.012
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
A detailed, reproducible synthesis of 1,1'-diaminocobaltocenium hexafluorophosphate is provided. The compound can be made on gram scales in several steps starting from 1,1'-dimethylcobaltocenium salts. The X-ray structures of 1,1'-diaminocobaltocenium hexalluorophosphate and a related 1,1'-diaminoferrocenium salt, are described. (C) 2004 Elsevier Ltd. All rights reserved.
引用
收藏
页码：2937 / 2942
页数：6
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