On the synthesis and characterization of ZnO/MgO nanocomposite by thermal evaporation technique

被引：8

作者：

Chhikara, Deepak ^{[1
]}

Srivatsa, K. M. K. ^{[1
]}

Muthusamy, Senthil Kumar ^{[1
]}

机构：

[1] CSIR Natl Phys Lab, Phys Energy Harvesting Div, New Delhi 110012, India

来源：

SOLID STATE SCIENCES | 2014年 / 37卷

关键词：

ZnO/MgO nanocomposite; Thermal evaporation; X-ray diffraction; Scanning electron microscopy; Photoluminescence; LOW-TEMPERATURE SYNTHESIS; ZNO; GROWTH; DEPOSITION; PRECURSOR; EMISSION;

D O I：

10.1016/j.solidstatesciences.2014.09.002

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

ZnO/MgO nanocomposites have been synthesized by an easy and cost effective thermal evaporation technique. Various growth temperatures ranging from 800 to 900 degrees C were tried. It is observed that the process temperature plays a key role in the formation of ZnO/MgO nanocomposite and the proper formation of ZnO/MgO nanocomposite occurs at 875 degrees C temperature as confirmed by X-ray diffraction studies. Scanning electron microscopic images indicate that the ZnO/MgO nanocomposite is formed as agglomerated nanoparticles distributed over a large area. Energy dispersive X-ray analyses also reveal that the Mg composition in the synthesized nanocomposite strongly depends on the process temperature. Photoluminescence (PL) spectrum exhibits a blue shift for the ZnO/MgO nanocomposite synthesized at 875 degrees C indicating the incorporation of Mg into the ZnO crystal lattice. A higher PL intensity ratio of band-edge to deep band emission has been observed for this sample indicating the presence of low crystalline defects. (C) 2014 Elsevier Masson SAS. All rights reserved.

引用

页码：108 / 113

页数：6

共 28 条

[11] CRYSTAL-GROWTH IN C DIRECTION AND CRYSTALLOGRAPHIC POLARITY IN ZNO CRYSTALS [J].

IWANAGA, H ;

SHIBATA, N ;

NITTONO, O ;

KASUGA, M .

JOURNAL OF CRYSTAL GROWTH, 1978, 45 (01) :228-232

[12] Fabrication and characterization of vertically aligned ZnMgO/ZnO nanowire arrays [J].

Kar, J. P. ;

Jeong, M. C. ;

Lee, W. K. ;

Myoung, J. M. .

MATERIALS SCIENCE AND ENGINEERING B-SOLID STATE MATERIALS FOR ADVANCED TECHNOLOGY, 2008, 147 (01) :74-78

[13]

Karimi MA, 2011, Int. Nano Lett., V1, P43

[14] Growth of self-assembled ZnO rods cellular network over a large area by thermal evaporation method [J].

Kumar, M. Senthil ;

Chhikara, Deepak ;

Srivatsa, K. M. K. .

MATERIALS LETTERS, 2011, 65 (12) :1938-1940

[15] Low-temperature synthesis of novel ZnO nanowire microspheres on silicon substrates [J].

Li Xinyu ;

Guo Jian ;

Ding Shulong ;

Lin Tiejun ;

Dong Jingtao .

RARE METALS, 2007, 26 (03) :242-246

[16] The deposition and annealing study of MOCVD ZnMgO [J].

Liu, W ;

Gu, SL ;

Zhu, SM ;

Ye, JD ;

Qin, F ;

Liu, SM ;

Zhou, X ;

Hu, LQ ;

Zhang, R ;

Shi, Y ;

Zheng, YD .

JOURNAL OF CRYSTAL GROWTH, 2005, 277 (1-4) :416-421

[17] Synthesis and Characterization of Brush-Like ZnO Nanorods using Albumen as Biotemplate [J].

Nouroozi, Fatemeh ;

Farzaneh, Faezeh .

JOURNAL OF THE BRAZILIAN CHEMICAL SOCIETY, 2011, 22 (03) :484-488

[18] MgxZn1-xO as a II-VI widegap semiconductor alloy [J].

Ohtomo, A ;

Kawasaki, M ;

Koida, T ;

Masubuchi, K ;

Koinuma, H ;

Sakurai, Y ;

Yoshida, Y ;

Yasuda, T ;

Segawa, Y .

APPLIED PHYSICS LETTERS, 1998, 72 (19) :2466-2468

[19]

Samerjai T., 2009, J MICROSC SOC THAILA, V23, P87

[20] Use of chemically synthesized ZnO thin film as a liquefied petroleum gas sensor [J].

Shinde, V. R. ;

Gujar, T. P. ;

Lokhande, C. D. ;

Mane, R. S. ;

Han, Sung-Hwan .

MATERIALS SCIENCE AND ENGINEERING B-SOLID STATE MATERIALS FOR ADVANCED TECHNOLOGY, 2007, 137 (1-3) :119-125

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