Nitrogen-rich hypergolic ionic salts based on (2-methyltetrazol-5-yl)diazotates

被引：19
|
作者：
Wang, Qi [1 ]
Lu, Huijie [1 ]
Pang, Fuqing [1 ]
Huang, Jinglun [2 ]
Nie, Fude [2 ]
Chen, Fu-Xue [1 ]
机构：
[1] Beijing Inst Technol, Sch Chem Engn & Environm, 5 South Zhongguancun St, Beijing 100081, Peoples R China
[2] China Acad Engn Phys, Inst Chem Mat, Mianyang 621050, Sichuan, Peoples R China
来源：
RSC ADVANCES | 2016年 / 6卷 / 62期
关键词：
LIQUIDS; FUELS; PROPELLANTS;
D O I：
10.1039/c6ra11494f
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A series of hypergolic (2-methyltetrazol-5-yl)diazotates have been synthesized by treatment of bases with the diazotatic acid, which were prepared by using isoamyl nitrite at low temperature. These hypergolic energetic salts showed remarkable short ignition delay times (IDs) by droplet test and a high specific impulse up to 291.2 s by calculation. All compounds were fully characterized using IR spectroscopy, H-1 and C-13 NMR spectroscopy and differential scanning calorimetry (DSC), and, in the case of aminoguanidinium(2-methyltetrazol-5-yl)diazotate (8) and diaminoguanidinium (2-methyltetrazol-5-yl)diazotate (9), with single crystal X-ray structuring.
引用
收藏
页码：S6827 / S6830
页数：4
相关论文
共 9 条
  • [1] Guanidinium Dicyanamide-Based Nitrogen-Rich Energetic Salts as Additives of Hypergolic Ionic Liquids
    Sun, Changgeng
    Tang, Shaokun
    ENERGY & FUELS, 2020, 34 (11) : 15068 - 15071
  • [2] RETRACTED: Guanidinium dicyanamide-based nitrogen-rich energetic salts as additives of hypergolic ionic liquids (Retracted Article)
    Sun, Changgeng
    Tang, Shaokun
    COMBUSTION AND FLAME, 2021, 226 : 243 - 247
  • [3] Energetic ionic salts based on nitrogen-rich heterocycles: A prospective study
    Swain, Pravat K.
    Singh, Haridwar
    Tewari, Surya P.
    JOURNAL OF MOLECULAR LIQUIDS, 2010, 151 (2-3) : 87 - 96
  • [4] Nitrogen-Rich Energetic Ionic Liquids Based on the N,N-Bis(1H-tetrazol-5-yl)amine Anion - Syntheses, Structures, and Properties
    Dong, Lin-Lin
    He, Ling
    Liu, Hang-Yu
    Tao, Guo-Hong
    Nie, Fu-De
    Huang, Ming
    Hu, Chang-Wei
    EUROPEAN JOURNAL OF INORGANIC CHEMISTRY, 2013, 2013 (28) : 5009 - 5019
  • [5] Structure-property relationships of energetic nitrogen-rich salts composed of triaminoguanidinium or ammonium cation and tetrazole-based anions
    Shao, Yuling
    Zhu, Weihua
    Xiao, Heming
    JOURNAL OF MOLECULAR GRAPHICS & MODELLING, 2013, 40 : 54 - 63
  • [6] Contributions to the Chemistry of N-Methylnitramine: Crystal Structure, Synthesis of Nitrogen-Rich Salts, and Reactions towards 2-Nitro-2-azapropyl Derivatives
    Kettner, Marcos A.
    Klapoetke, Thomas M.
    Mueller, Thomas G.
    Suceska, Muhamed
    EUROPEAN JOURNAL OF INORGANIC CHEMISTRY, 2014, (28) : 4756 - 4771
  • [7] Novel nitrogen-rich energetic macromolecules based on 3,6-dihydrazinyl-1,2,4,5-tetrazine
    Cohen, Adva
    Yan, Qi-Long
    Shlomovich, Avital
    Aizikovich, Alexander
    Petrutik, Natan
    Gozin, Michael
    RSC ADVANCES, 2015, 5 (129) : 106971 - 106980
  • [8] Synthesis and hypergolic properties of flammable ionic liquids based on the cyano (1H-1,2,3-triazole-1-yl) dihydroborate anion
    Wang, Zhi
    Jin, Yunhe
    Zhang, Wenquan
    Wang, Binshen
    Liu, Tianlin
    Zhang, Jiaheng
    Zhang, Qinghua
    DALTON TRANSACTIONS, 2019, 48 (18) : 6198 - 6204
  • [9] Solvent-free 1H-tetrazole, 1,2,5,6-tetrahydronicotinonitrile and pyrazole synthesis using quinoline based ionic fluoride salts (QuFs): thermal and theoretical studies
    Iqbal, Nafees
    Hashim, Jamshed
    Ali, Syed Abid
    al-Rashida, Mariya
    Alharthy, Rima D.
    Ahmad, Shakeel
    Khan, Khalid Mohammed
    Basha, Fatima Zahra
    Moin, Syed Tarique
    Hameed, Abdul
    RSC ADVANCES, 2015, 5 (115) : 95061 - 95072
1