71Ga and 31P solid state NMR:: a powerful tool for the characterization of the first gallium phosphonates

被引：44
作者：
Fredoueil, F
Massiot, D
Poojary, D
Bujoli-Doeuff, M
Clearfield, A
Bujoli, B
机构：
[1] UMR CNRS 6513, Organ Synth Lab, F-44322 Nantes 03, France
[2] Ctr Rech Phys Hautes Temp, UPR CNRS 4212, F-45071 Orleans, France
[3] Texas A&M Univ, Dept Chem, College Stn, TX 77843 USA
[4] UMR CNRS 6502, Inst Mat Nantes, F-44322 Nantes 03, France
来源：
CHEMICAL COMMUNICATIONS | 1998年 / 02期
关键词：
D O I：
10.1039/a705270g
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Two new gallium phosphonates Ga(OH)(O3PC2H4CO2H) . H2O 1 and Ga-3(OH)(3)(O3PC2H4CO2)(2) . 2H(2)O 2 are prepared and characterized, using P-31 MAS and Ga-71 static NMR spectroscopy, showing a good correspondence between the fitted NMR parameters and the crystallographic data.
引用
收藏
页码：175 / 176
页数：2
相关论文
共 23 条
  • [1] Alberti G, 1996, COMPREHENSIVE SUPRAM, P151
  • [2] CORRELATION BETWEEN AL-27-NMR AND GA-71-NMR CHEMICAL-SHIFTS
    BRADLEY, SM
    HOWE, RF
    KYDD, RA
    [J]. MAGNETIC RESONANCE IN CHEMISTRY, 1993, 31 (10) : 883 - 886
  • [3] BOND-VALENCE PARAMETERS OBTAINED FROM A SYSTEMATIC ANALYSIS OF THE INORGANIC CRYSTAL-STRUCTURE DATABASE
    BROWN, ID
    ALTERMATT, D
    [J]. ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 1985, 41 (AUG): : 244 - 247
  • [4] LAYERED METAL PHOSPHATES AND PHOSPHONATES - FROM CRYSTALS TO MONOLAYERS
    CAO, G
    HONG, HG
    MALLOUK, TE
    [J]. ACCOUNTS OF CHEMICAL RESEARCH, 1992, 25 (09) : 420 - 427
  • [5] CORRELATIONS BETWEEN P-31 NMR CHEMICAL-SHIFTS AND STRUCTURAL PARAMETERS IN CRYSTALLINE INORGANIC PHOSPHATES
    CHEETHAM, AK
    CLAYDEN, NJ
    DOBSON, CM
    JAKEMAN, RJB
    [J]. JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1986, (03) : 195 - 197
  • [6] Clark BG, 1996, RADIOSURG, V1, P268
  • [7] SYNTHESIS AND CATALYTIC PROPERTIES OF MANGANESE PORPHYRINS INCORPORATED INTO PHOSPHONATE NETWORKS
    DENIAUD, D
    SCHOLLHORN, B
    MANSUY, D
    ROUXEL, J
    BATTIONI, P
    BUJOLI, B
    [J]. CHEMISTRY OF MATERIALS, 1995, 7 (05) : 995 - 1000
  • [8] Synthesis and crystal structure of two members of a new type of layered compound: Copper(II) hydroxyphosphonates
    Drumel, S
    Janvier, P
    BujoliDoeuff, M
    Bujoli, B
    [J]. INORGANIC CHEMISTRY, 1996, 35 (20) : 5786 - 5790
  • [9] A SYNTHETIC GALLOPHOSPHATE MOLECULAR-SIEVE WITH A 20-TETRAHEDRAL-ATOM PORE OPENING
    ESTERMANN, M
    MCCUSKER, LB
    BAERLOCHER, C
    MERROUCHE, A
    KESSLER, H
    [J]. NATURE, 1991, 352 (6333) : 320 - 323
  • [10] ALUMINUM-GALLIUM SUBSTITUTION IN YTTRIUM GARNETS INVESTIGATED BY NMR
    GAUTIER, N
    MASSIOT, D
    FARNAN, I
    COUTURES, JP
    [J]. JOURNAL DE CHIMIE PHYSIQUE ET DE PHYSICO-CHIMIE BIOLOGIQUE, 1995, 92 (10) : 1843 - 1846
123