Synthesis of mesostructured tin oxide with neutral surfactant as a template in aqueous media

被引:17
作者
Zhou, SX
Lu, SM
Ke, YX
Li, JM [1 ]
机构
[1] Univ Sci & Technol China, Dept Phys Chem, Anhua 230026, Peoples R China
[2] Yancheng Technol Coll, Dept Chem Engn, Jiangsu 224003, Peoples R China
基金
中国国家自然科学基金;
关键词
mesostructured tin oxide; neutral surfactant; hydrated tin chloride; high surface area;
D O I
10.1016/S0167-577X(02)01355-1
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Mesostructured tin oxide with high specific surface area was synthesized in weak alkaline condition. The synthesis of the product was achieved using a neutral surfactant (dodecylamine: C12H25NH2) as template, and hydrated tin chloride C (SnCl4.5H(2)O) as inorganic precursor. Mesostructured SnO2 was characterized by powder X-ray diffraction (XRD), N-2 adsorption-desorption experiment. The BET surface area of the sample calcined at 300 degreesC is 359 m(2)/g, with an average pore diameter (BJH) of 21 Angstrom. (C) 2002 Elsevier Science B.V. All rights reserved.
引用
收藏
页码:2679 / 2681
页数:3
相关论文
共 12 条
  • [1] A NEW FAMILY OF MESOPOROUS MOLECULAR-SIEVES PREPARED WITH LIQUID-CRYSTAL TEMPLATES
    BECK, JS
    VARTULI, JC
    ROTH, WJ
    LEONOWICZ, ME
    KRESGE, CT
    SCHMITT, KD
    CHU, CTW
    OLSON, DH
    SHEPPARD, EW
    MCCULLEN, SB
    HIGGINS, JB
    SCHLENKER, JL
    [J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1992, 114 (27) : 10834 - 10843
  • [2] Voids in variable chemical surroundings: Mesoporous metal oxides
    Behrens, P
    [J]. ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH, 1996, 35 (05): : 515 - 518
  • [3] Preparation of mesoporous tin oxide for electrochemical applications
    Chen, FL
    Liu, ML
    [J]. CHEMICAL COMMUNICATIONS, 1999, (18) : 1829 - 1830
  • [4] IMPROVED STABILITY OF MCM-41 THROUGH TEXTURAL CONTROL
    COUSTEL, N
    DIRENZO, F
    FAJULA, F
    [J]. JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1994, (08) : 967 - 968
  • [5] ORDERED MESOPOROUS MOLECULAR-SIEVES SYNTHESIZED BY A LIQUID-CRYSTAL TEMPLATE MECHANISM
    KRESGE, CT
    LEONOWICZ, ME
    ROTH, WJ
    VARTULI, JC
    BECK, JS
    [J]. NATURE, 1992, 359 (6397) : 710 - 712
  • [6] Synthesis and characterization of mesostructured tin oxide with crystalline walls
    Qi, LM
    Ma, JM
    Cheng, HM
    Zhao, ZG
    [J]. LANGMUIR, 1998, 14 (09) : 2579 - 2581
  • [7] Non-siliceous mesostructured and mesoporous materials
    Schüth, F
    [J]. CHEMISTRY OF MATERIALS, 2001, 13 (10) : 3184 - 3195
  • [8] Supramolecular assembly of mesostructured tin oxide
    Severin, KG
    Abdel-Fattah, TM
    Pinnavaia, TJ
    [J]. CHEMICAL COMMUNICATIONS, 1998, (14) : 1471 - 1472
  • [9] VLAGAPPAN N, 1996, CHEM COMMUN, P1685
  • [10] Synthesis of mesostructured SnO2 with CTAB and hydrous tin chloride
    Wang, YD
    Ma, CL
    Sun, XD
    Li, HD
    [J]. MATERIALS LETTERS, 2001, 51 (04) : 285 - 288