Lead-free SrBi4Ti4O15 and Bi4Ti3O12 material fabrication using the microwave-assisted molten salt synthesis method

被引:22
作者
Hao, Hua [1 ]
Liu, Han-xing [1 ]
Liu, Yang [1 ]
Cao, Ming-he [1 ]
Ouyang, Shi-xi [1 ]
机构
[1] Wuhan Univ Technol, State Key Lab Adv Technol Mat Synth & Proc, Key Lab Silicate Mat Sci & Engn, Sch Mat Sci & Engn, Wuhan 430070, Peoples R China
关键词
D O I
10.1111/j.1551-2916.2007.01632.x
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
In this paper, the microwave-assisted molten salt method (MAMSS) and molten salt method (MSS) were used to synthesize SrBi4Ti4O15 (SBT). The phase constitution was determined by powder X-ray diffraction and the microstructure of powder was examined by scanning electron microscopy. In contrast to the conventional MSS method, MAMSS produces more distinct plate-like grains and synthesizes both SBT and Bi4Ti3O12 (BTO) at 600 degrees C with a 30-min soaking time. The increase of temperature and soaking time can make the plate-like grains of BTO more distinct.
引用
收藏
页码:1659 / 1662
页数:4
相关论文
共 18 条
[11]  
Lange N. A., 1992, LANGES HDB CHEM
[12]   Templated grain growth of textured piezoelectric ceramics [J].
Messing, GL ;
Trolier-McKinstry, S ;
Sabolsky, EM ;
Duran, C ;
Kwon, S ;
Brahmaroutu, B ;
Park, P ;
Yilmaz, H ;
Rehrig, PW ;
Eitel, KB ;
Suvaci, E ;
Seabaugh, M ;
Oh, KS .
CRITICAL REVIEWS IN SOLID STATE AND MATERIALS SCIENCES, 2004, 29 (02) :45-96
[13]   Synthesis of textured Bi5Ti3FeO15 and LaBi4Ti3FeO15 ferroelectric layered Aurivillius phases by molten-salt flux methods [J].
Porob, Digamber G. ;
Maggard, Paul A. .
MATERIALS RESEARCH BULLETIN, 2006, 41 (08) :1513-1519
[14]   Microwave heating of conductive powder materials [J].
Rybakov, KI ;
Semenov, VE ;
Egorov, SV ;
Eremeev, AG ;
Plotnikov, IV ;
Bykov, YV .
JOURNAL OF APPLIED PHYSICS, 2006, 99 (02)
[15]  
Tas AC, 2001, J AM CERAM SOC, V84, P295
[16]   Microwave-assisted synthesis and sintering of NZP compounds [J].
Vaidhyanathan, B ;
Agrawal, DK ;
Roy, R .
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 2004, 87 (05) :834-839
[17]   A novel approach for preparation of Zn2SiO4:Tb nanoparticles by sol-gel-microwave heating [J].
Yang, HM ;
Shi, JX ;
Gong, ML .
JOURNAL OF MATERIALS SCIENCE, 2005, 40 (22) :6007-6010
[18]   SrBi2Nb2O9 thin films crystallized using a low power microwave oven [J].
Zanetti, SM ;
Vasconcelos, JS ;
Vasconcelos, NSLS ;
Leite, ER ;
Longo, E ;
Varela, JA .
JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2004, 24 (06) :1597-1602