Lead-free SrBi4Ti4O15 and Bi4Ti3O12 material fabrication using the microwave-assisted molten salt synthesis method

被引:22
作者
Hao, Hua [1 ]
Liu, Han-xing [1 ]
Liu, Yang [1 ]
Cao, Ming-he [1 ]
Ouyang, Shi-xi [1 ]
机构
[1] Wuhan Univ Technol, State Key Lab Adv Technol Mat Synth & Proc, Key Lab Silicate Mat Sci & Engn, Sch Mat Sci & Engn, Wuhan 430070, Peoples R China
关键词
D O I
10.1111/j.1551-2916.2007.01632.x
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
In this paper, the microwave-assisted molten salt method (MAMSS) and molten salt method (MSS) were used to synthesize SrBi4Ti4O15 (SBT). The phase constitution was determined by powder X-ray diffraction and the microstructure of powder was examined by scanning electron microscopy. In contrast to the conventional MSS method, MAMSS produces more distinct plate-like grains and synthesizes both SBT and Bi4Ti3O12 (BTO) at 600 degrees C with a 30-min soaking time. The increase of temperature and soaking time can make the plate-like grains of BTO more distinct.
引用
收藏
页码:1659 / 1662
页数:4
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