Characterization of h-WO3 nanorods synthesized by hydrothermal process

被引：77
|
作者：
Salmaoui, S. [2 ]
Sediri, F. [1 ,2 ]
Gharbi, N. [2 ]
机构：
[1] Univ Tunis Elmanar, Fac Sci Tunis, Tunis 2092, Tunisia
[2] Univ Tunis, Lab Chim Matiere Condensee, IPEIT, Tunis, Tunisia
来源：
POLYHEDRON | 2010年 / 29卷 / 07期
关键词：
Tungsten oxide; Aniline; Hydrothermal synthesis; Nanorods; HEXAGONAL TUNGSTEN BRONZE; STRUCTURAL-CHARACTERIZATION; ELECTROCHROMIC PROPERTIES; OPTICAL-PROPERTIES; OXIDE NANORODS; WO3; NANORODS; FILMS; NANOPARTICLES; NANOSTRUCTURES; FABRICATION;
D O I：
10.1016/j.poly.2010.02.025
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
Hexagonal tungsten oxide nanorods have been synthesized by hydrothermal strategy using Na2WO4 center dot 2H(2)O as tungsten source, aniline and sulfate sodium as structure-directing templates. Techniques X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), high-resolution transmission electron microscopy (HRTEM), Fourier transform infrared spectroscopy (FTIR) and Raman spectroscopy have been used to characterize the structure, morphology and composition of the nanorods. The h-WO3 nanorods are up to 5 mu m in length, and 50-70 nm in diameter. (C) 2010 Elsevier Ltd. All rights reserved.
引用
收藏
页码：1771 / 1775
页数：5
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