Evaluation of TCS/ZnCl2 with acetic anhydride as an acetylating reagent for methylene ketones

被引：18

作者：

Elmorsy, SS ^{[1
]}

Badawy, DS ^{[1
]}

Khatab, TK ^{[1
]}

机构：

[1] Mansoura Univ, Fac Sci, Dept Chem, Mansoura, Egypt

来源：

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS | 2005年 / 180卷 / 01期

关键词：

(TCS); tetrachlorosilane;

D O I：

10.1080/104265090507920

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

A new route for the preparation of beta-diketones which. have applications in organic synthesis by the reaction of methylene ketones, acetic anhydride TCS and ZnCl2 in the solvent methylene chloride at room temperature produces the corresponding beta-diketones in excellent yield.

引用

收藏

页码：109 / 116

页数：8

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