Automation of a Procedure for the Experimental Investigation of Liquid-Liquid Phase Separation

被引：9

作者：

Sibirtsev, Stephan ^{[1
]}

Goebel, Clara Berinike ^{[1
]}

Jupke, Andreas ^{[1
]}

机构：

[1] Rhein Westfal TH Aachen, AVT FVT Dept Chem Engn, Fluid Proc Engn, Forckenbeckstr 51, D-52074 Aachen, Germany

来源：

CHEMIE INGENIEUR TECHNIK | 2019年 / 91卷 / 12期

关键词：

Automated data evaluation; Batch settling experiment; Liquid-liquid dispersion; Phase separation; Temperature influence;

D O I：

10.1002/cite.201900162

中图分类号：

TQ [化学工业];

学科分类号：

0817 ;

摘要：

Optimal design of a liquid-liquid settler requires experimental investigation on phase separation behavior of the used material system under the same operating conditions as in the technical application. Performing these experiments and evaluating the obtained data is highly time-consuming. To reduce manual effort, the procedure was largely automated. In this work, the experimental setup, the automated procedure, and its validation results at various operating temperatures are presented. The results show the suitability of the automated procedure and the influence of temperature on phase separation behavior of the liquid-liquid system 1-octanol/water.

引用

页码：1787 / 1793

页数：7

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