Multiscale characterization of shale pore-fracture system: Geological controls on gas transport and pore size classification in shale reservoirs

A sound understanding of the pore-fracture system across all scales provides an in-depth look at the intricate gas transport mechanisms in shale reservoirs. We performed a comprehensive multiscale characterization analysis on the Longmaxi shale samples using five complementary techniques: low-temperature gas (N2) adsorption (LTGA), mercury intrusion porosimetry (MIP), nuclear magnetic resonance (NMR), field emission scanning electron microscopy (FE-SEM), and X-ray computed tomography (CT) scanning. For pore size distribution (PSD) determination, LTGA (N2) analysis can detect small pores (2?300 nm sized), while MIP analysis is suitable for large pores or fractures ( 1000 nm), and seepage pores or fracture-pores (pore size 1000 nm). Although slippage pores dominate in terms of the total volumetric contribution of the Longmaxi shale, with a clear presence of adsorption pores, overall gas transport in shale is predominantly controlled by the seepage pores (fracture-pores), which constitute a very small portion of the total volume.