Structural characterization and dehydration kinetics of Kirka inderite mineral: Application of non-isothermal models

被引：14

作者：

Figen, Aysel Kantuerk ^{[1
]}

Yilmaz, Muege San ^{[1
]}

Piskin, Sabriye ^{[1
]}

机构：

[1] Yildiz Tech Univ, Dept Chem Engn, Istanbul, Turkey

来源：

MATERIALS CHARACTERIZATION | 2010年 / 61卷 / 06期

关键词：

Inderite; Characterization; Dehydration; Kinetics; Non-isothermal; Thermal analysis;

D O I：

10.1016/j.matchar.2010.03.009

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Coats-Redfern, Arrhenius, Ozawa, Kissinger, and Doyle non-isothermal kinetic models were used to calculate the dynamic kinetic parameters for dehydration reaction of Mg-borate mineral, inderite (Kirka - Turkey) based on thermogravimetric analysis, derivative thermogravimetric analysis and differential thermal analysis. Dehydration experiments were carried out at different heating rates of 2, 5, 10, 15, and 20 degrees C/min in a pure nitrogen atmosphere. Structural and morphological properties have been characterized by X-Ray diffraction, Fourier transform-infrared spectroscopy, Scanning electron microscopy-energy dispersive spectroscopy, and Inductively coupled plasma-optical emission spectroscopy techniques. (C) 2010 Elsevier Inc. All rights reserved.

引用

页码：640 / 647

页数：8

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