A Convenient Synthesis of 1,3,2-Benzodiazaphophorine-2-oxide

被引：5
|
作者：
Hichri, Sarra [1 ]
Abderrahim, Raoudha [1 ]
机构：
[1] Univ Carthage, Fac Sci Bizerte, Lab Phys Lamellaires Mat & Hybrids Nanomat, Zarzouna 7021, Bizerte, Tunisia
来源：
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS | 2015年 / 190卷 / 01期
关键词：
Anthranilonitrile; hexamethylphosphoric triamide; diazaphosphorine-2-oxide; amidines; 2-OXIDES; DERIVATIVES;
D O I：
10.1080/10426507.2014.914931
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The reaction of amidines 1 with hexamethylphosphoric triamide in refluxing toluene is described as a simple and efficient method for the synthesis of 1,3,2-diazaphosphorine-2-oxide derivatives 3. The structures of all the synthesized compounds have been established by NMR (H-1, C-13, P-31) and IR spectroscopy, as well as by elemental analysis and in the case of 3d by MS spectral data.
引用
收藏
页码：29 / 35
页数：7
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