Synthesis of β-AgVO3 nanowires by hydrothermal and precipitation routes: a comparative study

被引:16
作者
Canuto de Menezes, Beatriz Rossi [1 ]
Ribas, Renata Guimaraes [1 ]
Schatkoski, Vanessa Modelski [1 ]
do Amaral Montanheiro, Thais Larissa [1 ]
Koga-Ito, Cristiane Yumi [2 ]
Thim, Gilmar Patrocinio [1 ]
机构
[1] Inst Tecnol Aeronaut, LPP, Praca Marechal Eduardo Gomes 50, BR-12228970 Sao Jose Dos Campos, SP, Brazil
[2] Univ Estadual Paulista, UNESP, Lab Genoma, Inst Ciencia & Tecnol, Campus Sao Jose dos Campos ICT, BR-12247016 Sao Jose Dos Campos, SP, Brazil
来源
SN APPLIED SCIENCES | 2019年 / 1卷 / 11期
关键词
Silver vanadate; beta-AgVO3; Precipitation synthesis; Hydrothermal method; IN-SITU RAMAN; FACILE SYNTHESIS; AGVO3; NANOWIRES; SILVER; HYBRID; NANORIBBONS; SCATTERING; STABILITY; AG2V4O11; NANORODS;
D O I
10.1007/s42452-019-1396-1
中图分类号
O [数理科学和化学]; P [天文学、地球科学]; Q [生物科学]; N [自然科学总论];
学科分类号
07 ; 0710 ; 09 ;
摘要
Silver vanadate, especially beta-AgVO3, have a wide range of technological applications due to remarkable biological, optical, and electrical features. The structure, morphology, and properties of beta-AgVO3 are directly affected by synthesis conditions. A comparative study between two different synthesis routes (precipitation and hydrothermal) of beta-AgVO3 was systematically investigated in this work. X-ray diffraction, Raman spectroscopy, scanning electron microscopy, zeta potential, and UV-visible spectrometry results showed that the hydrothermal method produced more homogeneous samples of beta-AgVO3, with elevated purity and crystallinity. In addition, the sample of beta-AgVO3 obtained by hydrothermal method had a wire-like morphology while that obtained by precipitation had irregular shape. Finally, the hydrothermal procedure showed more elevated reproducibility.
引用
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页数:8
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