An efficient and rapid one-pot synthesis of highly functionalized stable phosphorus ylides containing the sulfur atom

被引：24
|
作者：
Islami, MR [1 ]
Hassani, Z [1 ]
Saidi, K [1 ]
机构：
[1] Shahid Bahonar Univ Kerman, Dept Chem, Kerman 76175133, Iran
来源：
SYNTHETIC COMMUNICATIONS | 2003年 / 33卷 / 01期
关键词：
D O I：
10.1081/SCC-120015560
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
A one-pot synthesis of stable ylides by reaction of triphenyl-phosphine, dialkyl acetylenedicarboxylates and strong S-H acids, such as thiophenol or 4-fluorothiophenol in good to excellent yields is reported. The phosphoranes exhibit a mixture of rotational isomers in the ratio of 1:1 at ambient temperature.
引用
收藏
页码：65 / 72
页数：8
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