SOLVENT-FREE SYNTHESIS OF N-ARYLFULLEROPYRROLIDINE DERIVATIVES WITHOUT USING PHASE-TRANSFER CATALYST UNDER MICROWAVE IRRADIATION

被引：5

作者：

Jin, Bo ^{[1
,2
]}

Peng, Ru-Fang ^{[1
]}

Yang, Wen-Ning ^{[1
]}

Wang, Kai ^{[1
]}

Yuan, Bang-Qun ^{[1
]}

Chu, Shi-Jin ^{[1
]}

机构：

[1] SW Univ Sci & Technol, Sch Mat Sci & Engn, Mianyang 621010, Sichuan, Peoples R China

[2] Beijing Inst Technol, Sch Chem Engn & Environm, Beijing 100081, Peoples R China

来源：

SYNTHETIC COMMUNICATIONS | 2010年 / 40卷 / 04期

基金：

中国国家自然科学基金;

关键词：

N-Arylation; fullerene; fulleropyrrolidine; microwave irradiation; solvent-free; FULLERENE CHEMISTRY; C-60; FULLEROPYRROLIDINES;

D O I：

10.1080/00397910903007061

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Several N-arylfulleropyrrolidine derivatives were synthesized via the direct solvent-free reactions of N-unsubstituted fulleropyrrolidines and nitrochlorobenzenes under microwave irradiation in the absence of phase-transfer catalysts. Their structures were confirmed by ultraviolet-visble, Fourier transform-infrared, 1H NMR, and mass spectrometry.

引用

页码：580 / 586

页数：7

共 50 条

[41] Copper (I) bromide (CuBr): a highly efficient catalyst for the synthesis of β-enaminone derivatives using ultrasound irradiation under solvent-free conditions [J].

Redjemia, Rayenne ;

Bouzina, Abdeslem ;

Bouone, Yousra Ouafa ;

Mansouri, Achraf ;

Bahadi, Rania ;

Berredjem, Malika .

RESEARCH ON CHEMICAL INTERMEDIATES, 2022, 48 (12) :4947-4962

[42] Solvent-Free Fmoc Protection of Amines Under Microwave Irradiation [J].

Godoi, Marcelo ;

Botteselle, Giancarlo V. ;

Rafique, Jamal ;

Rocha, Manuela S. T. ;

Pena, Jesus M. ;

Braga, Antonio L. .

ASIAN JOURNAL OF ORGANIC CHEMISTRY, 2013, 2 (09) :746-749

[43] Microwave-Assisted Catalyst-Free and Solvent-Free Method for the Synthesis of Quinoxalines [J].

Zhou, Jian-Feng ;

Gong, Gui-Xia ;

Zhi, San-Jun ;

Duan, Xiu-Li .

SYNTHETIC COMMUNICATIONS, 2009, 39 (20) :3743-3754

[44] Solvent free synthesis of 2-aminothiazole derivatives under microwave irradiation [J].

Cheng, CY ;

Jiang, FC .

CHINESE JOURNAL OF ORGANIC CHEMISTRY, 2005, 25 (07) :826-829

[45] An efficient and solvent-free one-pot synthesis of dihydropyrimidinones under microwave irradiation [J].

Cheng Jiang Qi Dong You Department of Medicinal Chemistry China Pharmaceutical University Nanjing China .

Chinese Chemical Letters, 2007, (06) :647-650

[46] Solvent-Free Synthesis of Phthalimide Under Microwave Irradiation and Modification of Talc with Synthesized Phthalimide [J].

Cai, Yan-Hua .

ASIAN JOURNAL OF CHEMISTRY, 2012, 24 (02) :481-484

[47] A new solvent-free synthesis of α,α′-dibenzylidenecycloalkanones from acetals with cycloalkanones under microwave irradiation [J].

Huang, DF ;

Wang, JX ;

Hu, YL .

CHINESE CHEMICAL LETTERS, 2003, 14 (04) :333-334

[48] One-pot synthesis of iminoimidazolines under microwave irradiation in solvent-free conditions [J].

Servi, Sueleyman ;

Genc, Murat .

SYNTHETIC COMMUNICATIONS, 2007, 37 (18) :3173-3179

[49] An efficient and solvent-free one-pot synthesis of dihydropyrimidinones under microwave irradiation [J].

Jiang, Cheng ;

You, Qi Dong .

CHINESE CHEMICAL LETTERS, 2007, 18 (06) :647-650

[50] Multicomponent Solvent-Free Synthesis Of Benzimidazolyl Imidazo[1,2-a]-pyridine Under Microwave Irradiation [J].

Maiti, Barnali ;

Chanda, Kaushik ;

Selvaraju, Manikandan ;

Tseng, Chih-Chung ;

Sun, Chung-Ming .

ACS COMBINATORIAL SCIENCE, 2013, 15 (06) :291-297

← 1 2 3 4 5 →