Feedstock properties and debinding mechanism of yttria-stabilized zirconia/stainless steel 17-4PH micro-components fabricated via two-component micro-powder injection molding process

被引:15
作者
Al Basir [1 ]
Sulong, Abu Bakar [1 ]
Jamadon, Nashrah Hani [1 ]
Muhamad, Norhamidi [1 ]
机构
[1] Univ Kebangsaan Malaysia, Fac Engn & Built Environm, Dept Mech & Mfg Engn, Bangi 43600, Selangor, Malaysia
关键词
3YSZ; SS 17-4PH micro-parts; Two-component micro-powder injection mold-ing; Thermal properties; Debinding; Sintering; STAINLESS-STEEL; RHEOLOGICAL PROPERTIES; PEG/PMMA BINDER; PALM STEARIN; METAL; ZIRCONIA; MICROSTRUCTURE; OPTIMIZATION; BEHAVIOR; NITRIDE;
D O I
10.1016/j.ceramint.2021.04.057
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Two-component micro-powder injection molding (2C-mu PIM) is a promising technique to produce bi-material micro-sized components of 3 mol% yttria-stabilized zirconia (3YSZ) and 17-4PH stainless steel (SS 17-4PH). In this research, the solvent and thermal debinding mechanisms of the green 3YSZ/SS 17-4PH micro-parts were investigated using a systematic approach. For obtaining the feedstocks, 3YSZ and SS 17-4PH powders were individually mixed with palm stearin and low-density polyethylene (LDPE) binders. This experimental work revealed that the palm stearin elimination rate in 3YSZ/SS 17-4PH micro-parts consisted of 3YSZ and SS 17-4PH feedstocks with powder loadings of 44 vol% and 69 vol%, respectively, increased with an increase in the temperature during the solvent debinding process. While a substantial amount of palm stearin was removed from the interface and other regions of the bi-material micro-component at the solvent debinding temperature of 70 degrees C, the joining between 3YSZ and SS 17-4PH collapsed at 80 degrees C. The open channels that developed in the component solvent debound at 70 degrees C helped to eliminate 96%-99% of the binder system in the thermal debinding stage. After the sintering, the findings signified that bi-material micro-components could be fabricated successfully through the process route of 2C-mu PIM by using the feedstocks of 3YSZ and SS 17-4PH.
引用
收藏
页码:20476 / 20485
页数:10
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