The influence of perchloric acid on 2,3-dimethylpyrazine and 1,2-bis(4-pyridyl)ethane: crystal structure and Hirshfeld surfaces analysis

被引：1

作者：

Ling, Yang ^{[1
]}

Wang, Wei ^{[1
,2
]}

Yang, Li-Jing ^{[1
]}

Liu, Qing-Ling ^{[1
]}

Luo, Yang-Hui ^{[1
]}

Zhai, Li-Hai ^{[1
]}

Sun, Bai-Wang ^{[1
]}

机构：

[1] Southeast Univ, Sch Chem & Chem Engn, Nanjing 211189, Jiangsu, Peoples R China

[2] Southeast Univ, Coll Chengxian, Nanjing 210088, Jiangsu, Peoples R China

来源：

RESEARCH ON CHEMICAL INTERMEDIATES | 2016年 / 42卷 / 02期

基金：

中国国家自然科学基金;

关键词：

2,3-Dimethylpyrazine; 1,2-Bis(4-pyridyl) ethane; Hydrogen bonds; Hirshfeld surfaces; PHARMACEUTICAL COCRYSTALS; CO-CRYSTALS; COMPLEXES;

D O I：

10.1007/s11164-015-2049-7

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

2,3-Dimethylpyrazine and 1,2-bis(4-pyridyl)ethane are both N-containing aromatic heterocyclics with two N atoms approximately in the para position. We here report two compounds derived from these heterocyclics (compounds 1 and 2). Compounds 1 and 2 both form a 1:1 2,3-dimethylpyrazine:perchloric acid (PA) and 1,2-bis(4-pyridyl)ethane:PA cocrystal, respectively. Their crystal structures were characterized by single-crystal X-ray diffraction, which revealed that the C-Ha <-O and N-Ha <-O hydrogen bonding interactions were found to stabilize the crystal structure in compounds 1 and 2. However, PA plays a necessary role for the one-dimensional structure in 1 and the three-dimensional structure in 2. Hirshfeld surfaces and fingerprint plots were applied to get the same conclusion.

引用

页码：673 / 685

页数：13

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