Zinc oxide nanocones as potential scaffold for the fabrication of ultra-high sensitive hydrazine chemical sensor

被引:45
作者
Kumar, Sandeep [1 ]
Bhanjana, Gaurav [1 ]
Dilbaghi, Neeraj [1 ]
Umar, Ahmad [2 ,3 ]
机构
[1] Guru Jambheshwar Univ Sci & Technol, Dept Bio & Nano Technol, Hisar 125001, Haryana, India
[2] Najran Univ, Fac Sci & Arts, Dept Chem, Najran 11001, Saudi Arabia
[3] Najran Univ, PCSED, Najran 11001, Saudi Arabia
关键词
Electron microscopy; Electrodes; Sensors; ZnO nanocones; Hydrazine; ZNO NANOPARTICLES; ELECTROCATALYTIC OXIDATION; ELECTROCHEMICAL SENSOR; HYBRID MATERIAL; CARBON; DEGRADATION; NANORODS; SURFACE; PROBE;
D O I
10.1016/j.ceramint.2014.10.154
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
The fabrication and characterization of ultra-high sensitive hydrazine chemical sensor based on zinc oxide (ZnO) nanocones are reported. The ZnO nanocones were synthesized by a low-temperature solution process and examined by various techniques in terms of their morphological, structural, compositional and optical properties. The studies revealed that the synthesized ZnO materials possessed good-crystallinity and defined nanocone morphologies and exhibited good optical properties. The hydrazine chemical sensor was fabricated on the amperometric principle and shows ultra-high sensitivity and low detection limit. The estimated sensitivity and detection limit of the fabricated hydrazine chemical sensor were 50 x 10(4) mu A mu M-1 cm(-2) and 0.01 mu M, respectively. The observed response time was < 2 S. (C) 2014 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
引用
收藏
页码:3101 / 3108
页数:8
相关论文
共 49 条
[1]   n-ZnO Based Nanostructure/p-Silicon Substrate Based Efficient p-n Heterojunction Diode [J].
Al-Heniti, S. ;
Umar, Ahmad ;
Badran, R. I. ;
Zaki, H. M. ;
Al-Hajry, A. .
SCIENCE OF ADVANCED MATERIALS, 2013, 5 (03) :301-307
[2]   Hydrazine chemical sensing by modified electrode based on in situ electrochemically synthesized polyaniline/graphene composite thin film [J].
Ameen, Sadia ;
Akhtar, M. Shaheer ;
Shin, Hyung Shik .
SENSORS AND ACTUATORS B-CHEMICAL, 2012, 173 :177-183
[3]  
[Anonymous], 2010, Metal oxide nanostructures and their applications
[4]   RESONANT RAMAN-SCATTERING IN ZNO [J].
CALLEJA, JM ;
CARDONA, M .
PHYSICAL REVIEW B, 1977, 16 (08) :3753-3761
[5]   Well-Crystalline ZnO Nanostructures for the Removal of Acridine Orange and Coomassie Brilliant Blue R-250 Hazardous Dyes [J].
Chaudhary, Ganga Ram ;
Saharan, Priya ;
Umar, Ahmad ;
Mehta, S. K. ;
Mor, Suman .
SCIENCE OF ADVANCED MATERIALS, 2013, 5 (12) :1886-1894
[6]   TICT based fluorescence "turn-on" hydrazine probes [J].
Chen, Bin ;
Sun, Xi ;
Li, Xin ;
Agren, Hans ;
Xie, Yongshu .
SENSORS AND ACTUATORS B-CHEMICAL, 2014, 199 :93-100
[7]   Electrochemical sensor for detection of hydrazine based on Au@Pd core-shell nanoparticles supported on amino-functionalized TiO2 nanotubes [J].
Chen, Xianlan ;
Liu, Wei ;
Tang, Lele ;
Wang, Jian ;
Pan, Haibo ;
Du, Min .
MATERIALS SCIENCE & ENGINEERING C-MATERIALS FOR BIOLOGICAL APPLICATIONS, 2014, 34 :304-310
[8]   Highly selective amperometric sensor for the trace level detection of hydrazine at bismuth nanoparticles decorated graphene nanosheets modified electrode [J].
Devasenathipathy, Rajkumar ;
Mani, Veerappan ;
Chen, Shen-Ming .
TALANTA, 2014, 124 :43-51
[9]   A novel hydrazine electrochemical sensor based on a carbon nanotube-wired ZnO nanoflower-modified electrode [J].
Fang, Bin ;
Zhang, Cuihong ;
Zhang, Wei ;
Wang, Guangfeng .
ELECTROCHIMICA ACTA, 2009, 55 (01) :178-182
[10]   Integrated metabonomic analysis of the multiorgan effects of hydrazine toxicity in the rat [J].
Garrod, S ;
Bollard, ME ;
Nichollst, AW ;
Connor, SC ;
Connelly, J ;
Nicholson, JK ;
Holmes, E .
CHEMICAL RESEARCH IN TOXICOLOGY, 2005, 18 (02) :115-122