Microwave-Assisted Synthesis of NiO/C and Its Capacitance Property

被引：0

作者：

Zhang Chuanxiang ^{[1
,2
]}

Dai Yuming ^{[1
]}

He Xiancong ^{[1
]}

Ba Zhixin ^{[1
]}

Zhou Hengzhi ^{[1
]}

机构：

[1] Nanjing Inst Technol, Nanjing 211167, Jiangsu, Peoples R China

[2] Jiangsu Key Lab Adv Struct Mat & Applicat Technol, Nanjing 211167, Jiangsu, Peoples R China

来源：

RARE METAL MATERIALS AND ENGINEERING | 2016年 / 45卷 / 05期

基金：

中国国家自然科学基金;

关键词：

microwave irradiation; NiO/C; quantificational support; specific capacitance; ORDERED MESOPOROUS CARBONS; NICKEL-OXIDE; ELECTROCHEMICAL SUPERCAPACITOR; COMPOSITE ELECTRODES; METAL; CMK-3; NANOSTRUCTURE; NANOPARTICLES; PERFORMANCE; XPS;

D O I：

暂无

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Samples of OMC (ordered mesoporous carbon) and xNiO (x=0.01, 0.12, 0.04)/C composites were prepared by microwave assisted synthesis. X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), transmission electron microscopy (TEM), nitrogen adsorption, inductively coupled plasma (ICP) and cyclic voltammetry (CV) were employed to characterize the physical and chemical properties of the samples. Results show that slightly reducing of pore size means that nanoparticles are embedded on pore walls of OMC. However, OMC retaining of ordered mesostructure and large surface area upon supporting appropriate NiO content are confirmed by XRD, TEM and nitrogen sorption. Data of ICP show high supporting efficiency in the microwave -assisted method. Great specific capacitance over 400 F.g(-1) and high electrochemical stability present favorable prospects for this supporting method.

引用

页码：1093 / 1099

页数：7

共 31 条

[1] Synthesis, characterization, and electrochemical properties of ordered mesoporous carbons containing nickel oxide nanoparticles using sucrose and nickel acetate in a silica template [J].

Cao, Yulin ;

Cao, Jieming ;

Zheng, Mingbo ;

Liu, Jinsong ;

Ji, Guangbin .

JOURNAL OF SOLID STATE CHEMISTRY, 2007, 180 (02) :792-798

[2] Identification and functional analysis of the cytolethal distending toxin gene from Avibacterium paragallinarum [J].

Chen, Y-C ;

Tan, D-H ;

Shien, J-H ;

Hsieh, M-K ;

Yen, T-Y ;

Chang, P-C .

AVIAN PATHOLOGY, 2014, 43 (01) :43-50

[3] A structure of MnO2 embedded in CMK-3 framework developed by a redox method [J].

Dong, XP ;

Shen, WH ;

Gu, JL ;

Xiong, LM ;

Zhu, YF ;

Li, H ;

Shi, JL .

MICROPOROUS AND MESOPOROUS MATERIALS, 2006, 91 (1-3) :120-127

[4] MnO2-embedded-in-mesoporous-carbon-wall structure for use as electrochemical capacitors [J].

Dong, XP ;

Shen, WH ;

Gu, JL ;

Xiong, LM ;

Zhu, YF ;

Li, Z ;

Shi, JL .

JOURNAL OF PHYSICAL CHEMISTRY B, 2006, 110 (12) :6015-6019

[5] Microwave-assisted synthesis of metal oxide/hydroxide composite electrodes for high power supercapacitors - A review [J].

Faraji, Soheila ;

Ani, Farid Nasir .

JOURNAL OF POWER SOURCES, 2014, 263 :338-360

[6] Application of impregnation combustion method for fabrication of nanostructure CuO/ZnO composite oxide: XRD, FESEM, DRS and FTIR study [J].

Habibi, Mohammad Hossein ;

Karimi, Bahareh .

JOURNAL OF INDUSTRIAL AND ENGINEERING CHEMISTRY, 2014, 20 (04) :1566-1570

[7] Preparation and characterization of high metal content Pt-Ru alloy catalysts on various carbon blacks for DMFCs [J].

Han, Kookil ;

Lee, Jaeseung ;

Kim, Hasuck .

ELECTROCHIMICA ACTA, 2006, 52 (04) :1697-1702

[8] Synthesis and characterization of transition metal and metal oxide nanoparticles inside mesoporous carbon CMK-3 [J].

Huwe, Holger ;

Froeba, Michael .

CARBON, 2007, 45 (02) :304-314

[9] Electrochemical capacitor performance of hydrous ruthenium oxide/mesoporous carbon composite electrodes [J].

Jang, JH ;

Han, S ;

Hyeon, T ;

Oh, SM .

JOURNAL OF POWER SOURCES, 2003, 123 (01) :79-85

[10] A novel method to prepare nanostructured manganese dioxide and its electrochemical properties as a supercapacitor electrode [J].

Jiang, Rongrong ;

Huang, Tao ;

Liu, Jiali ;

Zhuang, Jihua ;

Yu, Aishui .

ELECTROCHIMICA ACTA, 2009, 54 (11) :3047-3052

← 1 2 3 4 →