Supercritical fluid extraction in isolation of cyclitols and sugars from chamomile flowers

被引：31

作者：

Al-Suod, Hossam ^{[1
,2
]}

Ratiu, Ileana-Andreea ^{[1
,2
,3
]}

Krakowska-Sieprawska, Aneta ^{[2
]}

Lahuta, Leslaw ^{[4
]}

Gorecki, Ryszard ^{[4
]}

Buszewski, Boguslaw ^{[1
,2
]}

机构：

[1] Nicolaus Copernicus Univ, Interdisciplinary Ctr Modern Technol, Wilenska 4, PL-87100 Torun, Poland

[2] Nicolaus Copernicus Univ, Dept Environm Chem & Bioanalyt, Fac Chem, Torun, Poland

[3] Babes Bolyai Univ, Fac Chem & Chem Engn, Cluj Napoca, Romania

[4] Univ Warmia & Mazury, Dept Plant Physiol Genet & Biotechnol, Olsztyn, Poland

来源：

JOURNAL OF SEPARATION SCIENCE | 2019年 / 42卷 / 20期

关键词：

chamomile; cyclitols isolation; response surface methodology; sugars isolation; supercritical fluid extraction; BIOACTIVE COMPOUNDS; PARTS;

D O I：

10.1002/jssc.201900539

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

The aim of the present study was to develop an optimization procedure for supercritical fluid extraction parameters, in order to obtain the highest possible yield of sugars and cyclitols from plant material. Response surface methodology based on Box-Behnken design was applied to evaluate the effect of: temperature (40, 60, 80 degrees C), pressure (100, 200, 300 bar), and co-solvent (methanol) percentage (20, 25, 30%). As a result of the optimization process, we found that the highest amount of sugars (15.02 mg/gof dried material) and cyclitols (0.86 mg/g of dried material) was obtained when the following parameters were applied: 80 degrees C, 228 bar, and 30% of methanol. Moreover, co-solvent concentration and temperature had a higher influence onto the obtained amounts compared with the pressure.

引用

页码：3243 / 3252

页数：10

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