Synthesis of novel chiral stationary phases for high-performance liquid chromatography

被引：4
|
作者：
Tan, Xu Lin [1 ]
Hou, Shi Cong [1 ]
Bian, Qing Hua [1 ]
Wang, Min [1 ]
机构：
[1] China Agr Univ, Coll Sci, Beijing 100094, Peoples R China
来源：
CHINESE CHEMICAL LETTERS | 2007年 / 18卷 / 04期
基金：
中国国家自然科学基金;
关键词：
enantioseparation; chiral stationary phase; amino acid derivatives; pyrethroid insecticides;
D O I：
10.1016/j.cclet.2007.02.010
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Three novel chiral selectors 4a-c were synthesized from (S)-amino acids and (R)-1-phenyl-2-(4-methylphenyl)ethylamine. 4a-c were connected to 3-aminopropylsilanized silica gel to be used as the chiral stationary phase for HPLC. Five amino acid derivatives and two pyrethroid insecticides were fairly resolved on these three new chiral stationary phases under normal phase condition. (c) 2007 Min Wang. Published by Elsevier B.V. on behalf of Chinese Chemical Society. All rights reserved.
引用
收藏
页码：461 / 464
页数：4
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