Influence of additives on size and porosity in the synthesis of uniform TiO2 nanoparticles

被引:5
作者
Widoniak, J [1 ]
Eiden-Assmann, S [1 ]
Maret, G [1 ]
机构
[1] Univ Konstanz, Fachbereich Phys, D-78457 Constance, Germany
来源
MESOPHASES, POLYMERS, AND PARTICLES | 2004年 / 129卷
关键词
titania particles; size and size distribution; thermogravimetry; tailoring particles; stabilizing polymer;
D O I
10.1007/b100312
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Monodisperse spherical titania particles of variable sizes are produced in a sol-gel synthesis from Ti(EtO)(4) in ethanol with addition of a salt or a polymer solution. The influence of different salt ions or polymer molecules on the size and on the size distribution of the final particles was investigated. The amorphous hydrous titania particles were characterized by electron microscopy, thermogravimetry, H-1-MAS-NMR and X-ray absorption spectroscopy and electrophoresis. Nitrogen absorption measurements revealed that the addition of polymers yields hollow and porous titania colloids.
引用
收藏
页码:119 / 125
页数:7
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