Crystal structure and Hirshfeld surface analysis of 4,5-dibromo-2-(4-methoxyphenyl)-2,3,4,4a,5,6,7,7a-octahydro-1H-4,6-epoxy-1H-cyclopenta[c]-pyridin-1-one

被引：0

作者：

Mertsalov, Dmitriy F. ^{[1
]}

Surina, Nataliya S. ^{[1
]}

Sorokina, Elena A. ^{[1
]}

Celikesir, Sevim Turktekin ^{[2
]}

Akkurt, Mehmet ^{[2
]}

Grigoriev, Mikhail S. ^{[3
]}

Mlowe, Sixberth ^{[4
]}

机构：

[1] Peoples Friendship Univ Russia, Dept Organ Chem, RUDN Univ, 6 Miklukho Maklaya St, Moscow 117198, Russia

[2] Erciyes Univ, Fac Sci, Dept Phys, TR-38039 Kayseri, Turkey

[3] Russian Acad Sci, Frumkin Inst Phys Chem & Electrochem, Leninskiy Prospect 31-4, Moscow 119071, Russia

[4] Univ Dar Es Salaam, Coll Educ, Dept Chem, POB 2329, Dar Es Salaam, Tanzania

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2021年 / 77卷

关键词：

crystal structure; epoxyisoindole group; hydrogen bond; halogen bond; non-covalent interactions; Hirshfeld surface analysis; CATALYTIC-ACTIVITY; BARBITURIC-ACID; CYANOSILYLATION; COMPLEXES; ARYLHYDRAZONE; COORDINATION; HALOGEN; OXIDATION; IRON(III); ALDEHYDES;

D O I：

10.1107/S2056989021003273

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The molecule of the title compound, C15H15Br2NO3, comprises a fused tricyclic system consisting of two five-membered rings (cyclopentane and tetrahydrofuran) and one six-membered ring (tetrahydropyridinone). Both five-membered rings of the tricyclic system have envelope conformations, and the conformation of the six-membered cycle is intermediate between chair and half-chair. In the crystal, the molecules are linked by C-H center dot center dot center dot O hydrogen bonds and C-H center dot center dot center dot pi, C-Br center dot center dot center dot pi and C center dot center dot center dot O interactions into double layers. The layers are connected into a three-dimensional network by van der Waals interactions.

引用

页码：532 / +

页数：10

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