Synthesis of CuS by elemental-direct-reaction in a reline deep eutectic solvent and its catalytic activity in the thermal decomposition of ammonium perchlorate

被引：5

作者：

Zeng, Ying ^{[1
]}

Yang, Fu ^{[1
]}

Liu, Chunsheng ^{[1
]}

Luo, Genxiang ^{[1
]}

机构：

[1] Liaoning Shihua Univ, Sch Chem & Mat Sci, Fushun 113001, Peoples R China

来源：

RESEARCH ON CHEMICAL INTERMEDIATES | 2016年 / 42卷 / 04期

关键词：

Deep eutectic solvent; Elemental-direct-reaction; CuS; Ammonium Aperchlorate; Thermal decomposition; ROOM-TEMPERATURE SYNTHESIS; COPPER SULFIDE; METAL CHALCOGENIDES; IONIC LIQUIDS; THIN-FILMS; NANOSTRUCTURES; NANOCRYSTALS; GROWTH; BATTERIES; TEMPLATE;

D O I：

10.1007/s11164-015-2212-1

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Micro-sized copper sulfide (CuS) has been successfully synthesized via an elemental-direct-reaction route in a reline deep eutectic solvent at a low temperature condition (50 A degrees C). The copper sulfide was characterized by X-ray diffraction pattern, scanning electron microscopy images, energy-dispersive X-ray spectroscopy, and transmission electron microscopy. The as-synthesized copper sulfide was pure hexagonal phase microspheres (about 4.0-4.3 mu m in diameter), which were assembled with randomly oriented thin slices (about 18 nm in thickness). Moreover, the CuS samples showed high catalytic activity for the thermal decomposition of ammonium perchlorate.

引用

页码：3315 / 3324

页数：10

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