Determining the Composition of Long-Flame Coal by Chemical and Instrumental Methods: A Comparison

被引:0
作者
Efimova, O. S. [1 ]
Panina, L. V. [1 ]
机构
[1] Russian Acad Sci, Inst Coal Chem & Chem Mat, Siberian Branch, Fed Res Ctr Coal & Coal Chem, Kemerovo, Russia
关键词
long-flame coal; elemental analysis; chemical composition; Eschka method; Kjeldahl method; instrumental method; high-temperature catalytic oxidation; statistical analysis;
D O I
10.3103/S1068364X22010021
中图分类号
TQ [化学工业];
学科分类号
0817 ;
摘要
For long-flame coal, the content of the basic elements in the organic mass (carbon, hydrogen, nitrogen, sulfur, and oxygen) is determined. Standard chemical methods are employed: accelerated determination of carbon and hydrogen; the Kjeldahl method for nitrogen; and the Eschka method for total sulfur. Their content is also determined by an instrumental method. The results are subjected to statistical analysis; the data from chemical and instrumental analysis are compared. For all the elements, the discrepancy is insignificant; the dispersion is uniform; and the results obtained by the methods may be regarded as equally accurate. On that basis, chemical coal analysis may be replaced by instrumental analysis, with considerable savings of time.
引用
收藏
页码:7 / 10
页数:4
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