N-(2-chloro-4-nitrophenyl)-N′-octanoylthiourea

被引:2
作者
Yusof, M. Sukeri M. [1 ]
Ramlee, Nurulain M.
Kadir, Maisara A.
Yamin, Bohari M.
机构
[1] Univ Malaysia Terengganu, Dept Chem Sci, Fac Sci & Technol, Kuala Terengganu 21030, Malaysia
[2] Univ Kebangsaan Malaysia, Sch Chem Sci & Food Technol, Bangi 43600, Selangor, Malaysia
关键词
D O I
10.1107/S1600536807017266
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The title compound, C15H20ClN3O3S, adopts a trans-cis configuration with respect to the positions of the octanoyl and 2-chloro-4-nitrophenyl groups relative to the S atom across their respective C-N bonds. Molecules exhibit intramolecular N-H center dot center dot center dot O hydrogen bonds and are linked into dimers through N-H center dot center dot center dot S interactions.
引用
收藏
页码:O2552 / O2553
页数:2
相关论文
共 7 条
[1]   TABLES OF BOND LENGTHS DETERMINED BY X-RAY AND NEUTRON-DIFFRACTION .1. BOND LENGTHS IN ORGANIC-COMPOUNDS [J].
ALLEN, FH ;
KENNARD, O ;
WATSON, DG ;
BRAMMER, L ;
ORPEN, AG ;
TAYLOR, R .
JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1987, (12) :S1-S19
[2]  
BRUKER, 1997, SHELXTL VERSION 5 1
[3]  
BRUKER, 2000, SADABS VERSION 2 01
[4]  
Nardelli M., 1995, J APPL CRYSTALLOGR, V28, P659, DOI DOI 10.1107/S0021889895007138
[5]  
Sheldrick G. M., 1997, SHELXS 97 PROGRAM CR, P38
[6]   Single-crystal structure validation with the program PLATON [J].
Spek, AL .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2003, 36 :7-13
[7]   N-hexanoyl-N′-(6-methyl-2-pyridyl)thiourea [J].
Yusof, M. Sukeri M. ;
Yaakob, Wan Nur Aishah ;
Kadir, Maisara A. ;
Yamin, Bohari M. .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 :O241-O243