ROMPGEL scavengers:: A high-loading supported anhydride for sequestering amines and hydrazines

被引:26
作者
Arnauld, T
Barrett, AGM [1 ]
Cramp, SM
Roberts, RS
Zécri, FJ
机构
[1] Univ London Imperial Coll Sci Technol & Med, Dept Chem, London SW7 2AY, England
[2] Aventis CropSci, Ongar CM5 0HW, Essex, England
关键词
D O I
10.1021/ol006191s
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
[GRAPHICS] A versatile method for sequestering excess amines and hydrazines is reported using a high loading ROMPGEL anhydride polymer.
引用
收藏
页码:2663 / 2666
页数:4
相关论文
共 32 条
[1]   PALLADIUM-CATALYZED PREPARATION OF EXO-ARYL DERIVATIVES OF THE NORBORNANE SKELETON [J].
ARCADI, A ;
MARINELLI, F ;
BERNOCCHI, E ;
CACCHI, S ;
ORTAR, G .
JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1989, 368 (02) :249-256
[2]   A ROMPGEL-supported N-hydroxysuccinimide:: A host of acylations with minimal purification [J].
Barrett, AGM ;
Cramp, SM ;
Roberts, RS ;
Zecri, FJ .
ORGANIC LETTERS, 2000, 2 (03) :261-264
[3]   Chromatography-free synthesis of 1,2,4-oxadiazoles using ROMPGEL-supported acylating reagents [J].
Barrett, AGM ;
Cramp, SM ;
Roberts, RS ;
Zécri, FJ .
COMBINATORIAL CHEMISTRY & HIGH THROUGHPUT SCREENING, 2000, 3 (02) :131-138
[4]   Horner-Emmons synthesis with minimal purification using ROMPGEL: A novel high-loading matrix for supported reagents [J].
Barrett, AGM ;
Cramp, SM ;
Roberts, RS ;
Zecri, FJ .
ORGANIC LETTERS, 1999, 1 (04) :579-582
[5]   Solid-supported reagent strategies for rapid purification of combinatorial synthesis products [J].
Booth, RJ ;
Hodges, JC .
ACCOUNTS OF CHEMICAL RESEARCH, 1999, 32 (01) :18-26
[6]   Polymer-supported quenching reagents for parallel purification [J].
Booth, RJ ;
Hodges, JC .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1997, 119 (21) :4882-4886
[7]   Solid-phase organic reactions III: A review of the literature Nov 96 Dec 97 [J].
Booth, S ;
Hermkens, PHH ;
Ottenheijm, HCJ ;
Rees, DC .
TETRAHEDRON, 1998, 54 (51) :15385-15443
[8]   Ring-opening-metathesis polymerization for the preparation of carboxylic-acid-functionalized, high-capacity polymers for use in separation techniques [J].
Buchmeiser, MR ;
Atzl, N ;
Bonn, GK .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1997, 119 (39) :9166-9174
[9]  
BUNIN BA, 1998, COMBINATORIAL INDEX
[10]   A new scavenger resin for amines [J].
Coppola, GM .
TETRAHEDRON LETTERS, 1998, 39 (45) :8233-8236