A versatile experimental system for tracking ultrafast chemical reactions with X-ray free-electron lasers

被引：12

作者：

Katayama, Tetsuo ^{[1
,2
]}

Nozawa, Shunsuke ^{[3
,4
]}

Umena, Yasufumi ^{[5
,6
]}

Lee, SungHee ^{[7
,8
]}

Togashi, Tadashi ^{[1
,2
]}

Owada, Shigeki ^{[1
,2
]}

Yabashi, Makina ^{[2
]}

机构：

[1] Japan Synchrotron Radiat Res Inst, 1-1-1 Kouto, Sayo, Hyogo 6795198, Japan

[2] RIKEN, SPring 8 Ctr, 1-1-1 Kouto, Sayo, Hyogo 6795148, Japan

[3] High Energy Accelerator Res Org KEK, Inst Mat Struct Sci, 1-1 Oho, Tsukuba, Ibaraki 3050801, Japan

[4] Grad Univ Adv Studies, Sch High Energy Accelerator Sci, Dept Mat Struct Sci, 1-1 Oho, Tsukuba, Ibaraki 3050801, Japan

[5] Okayama Univ, Res Inst Interdisciplinary Sci, 3-1-1 Tshushima Naka, Okayama 7008530, Japan

[6] Okayama Univ, Grad Sch Nat Sci & Technol, 3-1-1 Tshushima Naka, Okayama 7008530, Japan

[7] Pusan Natl Univ, Dept Chem, Busan 609735, South Korea

[8] Pusan Natl Univ, Chem Inst Funct Mat, Busan 609735, South Korea

来源：

STRUCTURAL DYNAMICS-US | 2019年 / 6卷 / 05期

关键词：

EVOLVING PHOTOSYSTEM-II; STRUCTURAL-CHANGES; BOND FORMATION; DYNAMICS; SPECTROSCOPY; RESOLUTION;

D O I：

10.1063/1.5111795

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

An experimental system, SPINETT (SACLA Pump-probe INstrumEnt for Tracking Transient dynamics), dedicated for ultrafast pump-probe experiments using X-ray free-electron lasers has been developed. SPINETT consists of a chamber operated under 1 atm helium pressure, two Von Hamos spectrometers, and a large two-dimensional detector having a short work distance. This platform covers complementary X-ray techniques; one can perform time-resolved X-ray absorption spectroscopy, time-resolved X-ray emission spectroscopy, and time-resolved X-ray diffuse scattering. Two types of liquid injectors have been prepared for low-viscosity chemical solutions and for protein microcrystals embedded in a matrix. We performed a test experiment at SPring-8 Angstrom Compact free-electron LAser and demonstrated the capability of SPINETT to obtain the local electronic structure and geometrical information simultaneously. (C) 2019 Author(s). All article content, except where otherwise noted, is licensed under a Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).

引用

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