The study of Cistanche deserticola using Fourier transform infrared spectroscopy combined with two-dimensional correlation infrared spectroscopy

被引:4
作者
Lei, Yu [1 ]
Zhou, Qun [1 ]
Ya, Tu [1 ]
Chen, Jian-bo [1 ]
Sun, Su-qin [1 ]
Noda, Isao [2 ]
机构
[1] Tsinghua Univ, Key Lab Bioorgan Phosphorus Chem & Chem Biol, Minist Educ, Dept Chem,Anal Ctr, Beijing 100084, Peoples R China
[2] Procter & Gamble Co, W Chester, OH 45069 USA
关键词
Cistanche deserticola YC Ma; Infrared spectroscopy (IR); Two-dimensional infrared spectroscopy (2D-IR); GINSENG;
D O I
10.1016/j.molstruc.2010.03.020
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Infrared (IR) spectroscopy is used in combination with two-dimensional (2D) correlation IR spectroscopy to conduct rapid non-destructive quantitative research on extracts of Cistanche deserticola. In order to select the appropriate alcohol concentration to immerse the C. deserticola, we analyze the extracts of alcohol of different concentration with multi-steps. The findings indicate that FT-IR spectrum can provide many holistic variation rules of chemical constituents. The use of the macroscopical fingerprint characters of FT-IR and 2D-IR spectrum can, not only identify the main chemical constituents in C. deserticola, but also reveal the important spectroscopic fingerprint characteristics specific to the extracts prepared with 40-60% alcohol by volume, which contain more of the active constituents of C. deserticola. This analytical method is considerably rapid, effective and accurate for selecting the extracts prepared with appropriate alcohol concentration. (C) 2010 Elsevier B.V. All rights reserved.
引用
收藏
页码:156 / 160
页数:5
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