An NMR Spectral Study of the Structure of 5,5,6-trihydroxy-6-methyldihydropyrimidine-2,4-(1H,3H)-dione in DMSO-d6

被引：1
|
作者：
Petrova, S. F. [1 ]
Nugumanov, T. R. [1 ]
Lobov, A. N. [1 ]
Spirikhin, L., V [1 ]
Ivanov, S. P. [1 ]
机构：
[1] Russian Acad Sci, Ufa Fed Ctr, Ufa Inst Chem, Ufa, Russia
来源：
JOURNAL OF APPLIED SPECTROSCOPY | 2022年 / 89卷 / 02期
关键词：
5; 6-trihydroxy-6-methyldihydropyrimidine-2; 4(1H; 3H)-dione; NMR spectroscopy; dimethyl sulfoxide; EFFICIENT SCAVENGER; 5-HYDROXY-6-METHYLURACIL; OXIDATION;
D O I：
10.1007/s10812-022-01347-z
中图分类号：
O433 [光谱学];
学科分类号：
0703 ; 070302 ;
摘要：
The structure of 5,5,6-trihydroxy-6-methyldihydropyrimidine-2,4(1H,3H)-dione (2) was proven using C-13, H-1, and N-15 NMR spectroscopy. A new form (2a) was detected and shown to have a structure similar to dione 2.
引用
收藏
页码：225 / 231
页数：7
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