4-Chloro-N-(4-chlorobenzoyl)benzenesulfonamide

被引：7

作者：

Suchetan, P. A. ^{[1
]}

Gowda, B. Thimme ^{[1
]}

Foro, Sabine ^{[2
]}

Fuess, Hartmut ^{[2
]}

机构：

[1] Mangalore Univ, Dept Chem, Mangalore 574199, India

[2] Tech Univ Darmstadt, Inst Mat Sci, D-64287 Darmstadt, Germany

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷

关键词：

D O I：

10.1107/S160053681001559X

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C(13)H(9)Cl(2)NO(3)S, the conformation of the N-H bond in the C-SO(2)-NH-C(O) segment is anti to the C O bond. The molecule is twisted at the S atom with a torsion angle of 67.5 (3)degrees. The dihedral angle between the sulfonyl benzene ring and the -SO(2)-NH-C-O segment is 79.0 (1)degrees and that between the sulfonyl and benzoyl benzene rings is 85.6 (1)degrees. In the crystal, molecules are linked by N-H center dot center dot center dot O(S) hydrogen bonds with graph-set descriptor C(4) along the [010] direction.

引用

页码：O1253 / U83

页数：9

共 8 条

[1]

[Anonymous], 2009, CRYSALIS CCD CRYSALI

[2] PATTERNS IN HYDROGEN BONDING - FUNCTIONALITY AND GRAPH SET ANALYSIS IN CRYSTALS [J].

BERNSTEIN, J ;

DAVIS, RE ;

SHIMONI, L ;

CHANG, NL .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 1995, 34 (15) :1555-1573

[3]

Gowda B. T., 2009, ACTA CRYST E, VE65, po2516

[4] A short history of SHELX [J].

Sheldrick, George M. .

ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122

[5] Structure validation in chemical crystallography [J].

Spek, Anthony L. .

ACTA CRYSTALLOGRAPHICA SECTION D-STRUCTURAL BIOLOGY, 2009, 65 :148-155

[6] 2-Chloro-N-(2-chlorobenzoyl)benzenesulfonamide [J].

Suchetan, P. A. ;

Gowda, B. Thimme ;

Foro, Sabine ;

Fuess, Hartmut .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 :O1040-U1488

[7] N-Benzoyl-4-chlorobenzenesulfonamide [J].

Suchetan, P. A. ;

Gowda, B. Thimme ;

Foro, Sabine ;

Fuess, Hartmut .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 :O766-U1786

[8] N-(4-Chlorobenzoyl)benzenesulfonamide [J].

Suchetan, P. A. ;

Gowda, B. Thimme ;

Foro, Sabine ;

Fuess, Hartmut .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 :O3156-U1146

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