Hydrothermal extraction of α-Fe2O3 nanocrystallite from hematite ore

被引:18
|
作者
Khalil, N. M. [1 ,2 ]
Wahsh, M. M. S. [2 ]
Saad, Elhadi E. [3 ]
机构
[1] King Abdulaziz Univ, Fac Sci & Arts, Dept Chem, Khulais, Saudi Arabia
[2] Natl Res Ctr, Refractories Ceram & Bldg Mat Dept, Cairo, Egypt
[3] Sebha Univ, Fac Sci, Dept Chem, Sebha, Libya
关键词
Chemical reactions; alpha-Fe2O3; Powders; Nano materials; ONE-STEP SYNTHESIS; THERMAL-DECOMPOSITION; NANO-PARTICLES; BETA-FEOOH; MAGHEMITE; TRANSFORMATION; NANOPARTICLES;
D O I
10.1016/j.jiec.2014.05.037
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
alpha-Fe2O3 nanocrystallite has been extracted from its ore raw material by using simple chemical method. Mineralogical and chemical compositions of the raw material were investigated using X-ray diffraction (XRD), infrared (IR) and X-ray fluorescence (XRF) techniques. Also, thermal behavior including thermogravimetry (TG) and differential thermal analysis (DTA) of the raw material was examined. Scherrer's equation and XRD data were used to determinate the crystallite size and phase composition of the extracted hematite nanocrystallite. Morphology of the extracted alpha-Fe2O3 particles was tested using scanning electron microscope (SEM). About 96.80% of the total iron oxide present in the raw material sample was extracted as alpha-Fe2O3 with the average crystallite size less than 100 nm. The extracted alpha-Fe2O3 nanocrystallite is considered as a promise material for great technological applications as ceramic humidity sensors, catalysts, pigments, ferrofluid, recording systems, etc. (C) 2014 The Korean Society of Industrial and Engineering Chemistry. Published by Elsevier B.V. All rights reserved.
引用
收藏
页码:1214 / 1218
页数:5
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