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Simulation studies on homogenously catalyzed finishing reactive distillation for ethyl acetate production
被引:3
作者:
Singh, Damandeep
[1
]
Gupta, Raj Kumar
[2
]
Kumar, Vineet
[3
]
机构:
[1] IOL Chem & Pharmaceut Ltd, Barnala, Punjab, India
[2] Thapar Inst Engn & Technol, Dept Chem Engn, Patiala 147004, Punjab, India
[3] Indian Inst Technol ISM, Dept Chem Engn, Dhanbad, Bihar, India
关键词:
Equilibrium model;
esterification plant data;
ethyl acetate;
rate-based model;
reactive distillation;
DESIGN;
ESTERIFICATION;
KINETICS;
2-PHASE;
COLUMN;
MODEL;
D O I:
10.1080/00986445.2019.1574766
中图分类号:
TQ [化学工业];
学科分类号:
0817 ;
摘要:
A finishing reactive distillation (RD) column (50 stage), used for enhanced ethanol conversion, in an ethyl acetate production plant was simulated. This RD column followed a pre-reactor, wherein, homogeneously catalyzed esterification reaction for the production of ethyl acetate using acetic acid and ethanol was carried out. The simulation results of the RD column using equilibrium and rate-based models are compared with the plant data. The column design data for tray holdup, required for the rate-based model, was used. Effects of some design and operation parameters of the simulation results are also discussed.
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页码:109 / 122
页数:14
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