2-[2-(Methylamino)benzoyl]-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-1-one

被引：1

作者：

Li, Lin ^{[1
]}

Zhang, Yu-Tao ^{[1
]}

机构：

[1] Anshun Univ, Dept Chem Biol & Agr, Anshun 561000, Peoples R China

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷

关键词：

BOND;

D O I：

10.1107/S1600536810019409

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The title compound, C(19)H(17)N(3)O(2), was obtained from fruits of Evodia Rutaecarpa. In the solid state, the dihedral angle between the 2,3,4,9-tetrahydro-1H-pyrido[3,4-b] indol-1-one (tetrahydro-beta-carbolinone) unit and the benzoyl ring is 61.46 (3)degrees. In the crystal, dimers are formed through intermolecular N-H center dot center dot center dot O hydrogen-bonding interactions. In addition, intramolecular N-H center dot center dot center dot O hydrogen bonds are also observed. C-H center dot center dot center dot pi contacts connect the dimers, leading to the formation of a three-dimensional supramolecular network.

引用

页码：O1511 / U2288

页数：10

共 50 条

[11] Experimental and theoretical studies of the molecular structure of 4-(3-(1H-imidazol-1-yl)propyl)-5-p-tolyl-2H-1,2,4-triazol-3(4H)-one
Ustabas, Resat
Suleymanoglu, Nevin
Tanak, Hasan
Alpaslan, Yelda Bingol
Unver, Yasemin
Sancak, Kemal
JOURNAL OF MOLECULAR STRUCTURE, 2010, 984 (1-3) : 137 - 145
[12] Synthesis, characterisation and electrochemistry of eight Fe coordination compounds containing substituted 2-(1-(4-R-phenyl-1H-1,2,3-triazol-4-yl) pyridine ligands, R = CH3, OCH3, COOH, F, Cl, CN, H and CF3
Conradie, J.
Conradie, M. M.
Mtshali, Z.
van der Westhuizen, D.
Tawfiq, K. M.
Al-Jeboori, M. J.
Coles, S. J.
Wilson, C.
Potgieter, J. H.
INORGANICA CHIMICA ACTA, 2019, 484 (375-385) : 375 - 385
[13] The crystal structure of 1,4-bis(1,2,3,4,5-pentamethylcyclopenta-2,4-dien-1-yl)-3,6-bis ((4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)rnethylene)-1,4-dialuminacyclohexane benzene (1/2), C50H72Al2B2O4
Wang, Bing
Hu, Bo-Han
Wu, Di
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2022, : 119 - 121
[14] Organoantimony(III) compounds containing (imino)aryl ligands of the type 2-(RN=CH)C6H4 (R=2′,4′,6′-Me3C6H2, 2′,6′-iPr2C6H3): bromides and chalcogenides
Preda, Ana Maria
Rat, Ciprian I.
Silvestru, Cristian
Breunig, Hans J.
Lang, Heinrich
Rueffer, Tobias
Mehring, Michael
DALTON TRANSACTIONS, 2013, 42 (04) : 1144 - 1158
[15] Reactivity of triosmium clusters with 3,4-dimethyl-1-phenylphosphole and cyanoethyldi-tert-butylphosphine ligands: X-ray crystal structures of [Os3(CO)9(μ-OH)(μ-H)(η1-PhPC4H2Me2)] and [Os3(CO)11(η1- t Bu2PC2H4CN)]
Otero, Yomaira
Pena, Deisy
De Sanctis, Ysaura
Arce, Alejandro
Ocando-Mavarez, Edgar
Machado, Ruben
Gonzalez, Teresa
TRANSITION METAL CHEMISTRY, 2014, 39 (02) : 239 - 246
[16] Metal-Stabilized [B8H8]2- Derivatives with Dodecahedral Structure in the Solid and Solution States: [(Cp2MBH3)2B8H6] (Cp=η5-C5H5; M=Zr (1-Zr) and Hf (1-Hf)).
Kar, Sourav
Bairagi, Subhash
Joshi, Gaurav
Jemmis, Eluvathingal D.
Ghosh, Sundargopal
CHEMISTRY-A EUROPEAN JOURNAL, 2021, 27 (63) : 15634 - 15637
[17] DFT studies on tautomeric preferences. Part 3: Proton transfer in 2-(8-acylquinolin-2-yl)-1,3-diones
Dobosz, Robert
Osmialowski, Borys
Gawinecki, Ryszard
STRUCTURAL CHEMISTRY, 2010, 21 (05) : 1037 - 1041
[18] Crystal structure of 4-bromo-1H-imidazole, at 200 K, C3H3BrN2
Hosten, Eric C.
Betz, Richard
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2015, 230 (01): : 27 - 28
[19] Synthesis of 2-aryl-3-methylbenzo[g]indoles from 2-(arylethynyl)-1,8-bis(dimethylamino)naphthalenes: new examples of [1,3]-migration involving N-methyl group
Filatova, Ekaterina A.
Gulevskaya, Anna V.
Pozharskii, Alexander F.
CHEMISTRY OF HETEROCYCLIC COMPOUNDS, 2018, 54 (01) : 38 - 42
[20] The regulation mechanism of the excited-state behaviour of 3-Hydroxy-2-(1-ethyl-1H-pyrazol-3-yl)-4H-chromen-4-one fluorophore by solvent polarity: a computational study
Yang, Dapeng
Tian, Yanshan
Yang, Wenpeng
Zheng, Rui
MOLECULAR PHYSICS, 2022, 120 (10)

← 1 2 3 4 5 →