2-[2-(Methylamino)benzoyl]-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-1-one

被引:1
作者
Li, Lin [1 ]
Zhang, Yu-Tao [1 ]
机构
[1] Anshun Univ, Dept Chem Biol & Agr, Anshun 561000, Peoples R China
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷
关键词
BOND;
D O I
10.1107/S1600536810019409
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The title compound, C(19)H(17)N(3)O(2), was obtained from fruits of Evodia Rutaecarpa. In the solid state, the dihedral angle between the 2,3,4,9-tetrahydro-1H-pyrido[3,4-b] indol-1-one (tetrahydro-beta-carbolinone) unit and the benzoyl ring is 61.46 (3)degrees. In the crystal, dimers are formed through intermolecular N-H center dot center dot center dot O hydrogen-bonding interactions. In addition, intramolecular N-H center dot center dot center dot O hydrogen bonds are also observed. C-H center dot center dot center dot pi contacts connect the dimers, leading to the formation of a three-dimensional supramolecular network.
引用
收藏
页码:O1511 / U2288
页数:10
相关论文
共 11 条
[1]   TABLES OF BOND LENGTHS DETERMINED BY X-RAY AND NEUTRON-DIFFRACTION .1. BOND LENGTHS IN ORGANIC-COMPOUNDS [J].
ALLEN, FH ;
KENNARD, O ;
WATSON, DG ;
BRAMMER, L ;
ORPEN, AG ;
TAYLOR, R .
JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1987, (12) :S1-S19
[2]  
[Anonymous], 1998, REQAB
[3]   PATTERNS IN HYDROGEN BONDING - FUNCTIONALITY AND GRAPH SET ANALYSIS IN CRYSTALS [J].
BERNSTEIN, J ;
DAVIS, RE ;
SHIMONI, L ;
CHANG, NL .
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 1995, 34 (15) :1555-1573
[4]  
Johnson C. K., 1976, ORNL5138
[5]   A MILD NOVEL SYNTHESIS OF SIMPLE 1-OXO-BETA-CARBOLINES [J].
JOKELA, R ;
LOUNASMAA, M .
TETRAHEDRON, 1987, 43 (24) :6001-6006
[6]  
*RIG CORP, 1998, RAPID AUTO
[7]  
*RIG MSC, 2002, CRYSTALSTRUCTURE
[8]   A short history of SHELX [J].
Sheldrick, George M. .
ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122
[9]   Insertion of Isocyanides, Isothiocyanates, and Carbon Monoxide into the Pd-C Bond of Cyclopalladated Complexes Containing Primary Arylalkylamines of Biological and Pharmaceutical Significance. Synthesis of Lactams and Cyclic Amidinium Salts Related to the Isoquinoline, Benzo[g]isoquinoline, and β-Carboline Nuclei [J].
Vicente, Jose ;
Saura-Llamas, Isabel ;
Garcia-Lopez, Jose Antonio ;
Bautista, Delia .
ORGANOMETALLICS, 2009, 28 (02) :448-464
[10]   Stereoselective synthesis of (+)-isoindolo-β-carboline [J].
Wakchaure, Prasad B. ;
Puranik, Vedavati G. ;
Argade, Narshinha P. .
TETRAHEDRON-ASYMMETRY, 2009, 20 (02) :220-224