Solid-Phase Synthesis of Allosamidin

被引：18
|
作者：
Huang, Gang Liang [1 ]
Dai, Yue Peng [1 ]
机构：
[1] Chongqing Normal Univ, Coll Chem, Chongqing 400047, Peoples R China
来源：
SYNLETT | 2010年 / 10期
关键词：
allosamidin; solid-phase synthesis; trichloroacetimidate donors; Wang resin; glycosylation reactions;
D O I：
10.1055/s-0029-1219932
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
The solid-phase synthesis of allosamidin is described. After the NHCbz trichloroacetimidate donors were synthesized, solid-phase synthesis was performed using the Wang resin as support. The target allosamidin was obtained by iterative glycosylation reactions, catalytic hydrogenation, acetylation, and deacetylation, respectively.
引用
收藏
页码：1554 / 1556
页数：3
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