Microwave-assisted synthesis of group 6 (Cr, Mo, W) zerovalent organometallic carbonyl compounds

被引：44

作者：

VanAtta, SL ^{[1
]}

Duclos, BA ^{[1
]}

Green, DB ^{[1
]}

机构：

[1] Pepperdine Univ, Div Nat Sci, Malibu, CA 90263 USA

来源：

ORGANOMETALLICS | 2000年 / 19卷 / 12期

关键词：

D O I：

10.1021/om990977g

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The microwave-assisted synthesis of a series of compounds of the form ML(CO)(4) (M = Cr, Mo, W; L en, bipy, dppm, dppe), results in the reduction of reaction times and an increase in yields over previously published syntheses. Reaction times are reduced by a factor of 5 to over 500.

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页码：2397 / 2399

页数：3

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