Microwave-assisted synthesis of group 6 (Cr, Mo, W) zerovalent organometallic carbonyl compounds

被引:44
作者
VanAtta, SL [1 ]
Duclos, BA [1 ]
Green, DB [1 ]
机构
[1] Pepperdine Univ, Div Nat Sci, Malibu, CA 90263 USA
关键词
D O I
10.1021/om990977g
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
The microwave-assisted synthesis of a series of compounds of the form ML(CO)(4) (M = Cr, Mo, W; L en, bipy, dppm, dppe), results in the reduction of reaction times and an increase in yields over previously published syntheses. Reaction times are reduced by a factor of 5 to over 500.
引用
收藏
页码:2397 / 2399
页数:3
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