HEIMDAL: A thermal neutron powder diffractometer with high and flexible resolution combined with SANS and neutron imaging - Designed for materials science studies at the European Spallation Source

被引:10
作者
Holm, Sonja L. [1 ]
Lefmann, Kim [1 ]
Henry, Paul F. [2 ]
Bertelsen, Mads [1 ,2 ]
Schefer, Jurg [3 ]
Christensen, Mogens [4 ,5 ]
机构
[1] Univ Copenhagen, Niels Bohr Inst, Nanosci Ctr, Univ Pk 5, DK-2100 Copenhagen O, Denmark
[2] European Spallat Source ERIC, S-22100 Lund, Sweden
[3] Paul Scherrer Inst, Lab Neutron Scattering & Imaging, CH-5232 Villigen, Switzerland
[4] Aarhus Univ, Dept Chem, Langelandsgade 140, DK-8000 Aarhus C, Denmark
[5] Interdisciplinary Nanosci Ctr iNANO, Langelandsgade 140, DK-8000 Aarhus C, Denmark
基金
新加坡国家研究基金会;
关键词
ESS; Neutron instrumentation; McStas; Powder diffraction; SANS; Imaging; Materials science; In situ; TIME;
D O I
10.1016/j.nima.2016.05.046
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
HEIMDAL will be a multi length scale neutron scattering instrument for the study of structures covering almost nine orders of magnitude from 0.01 nm to 50 mm. The instrument is accepted for construction at the European Spallation Source (ESS) and features a variable resolution thermal neutron powder diffractometer (TNPD), combined with small angle neutron scattering (SANS) and neutron imaging (NI). The instrument uses a novel combination of a cold and a thermal guide to fulfill the diverse requirements for diffraction and SANS. With an instrument length of 170 m, HEIMDAL will take advantage of the high neutron flux of the long pulse at ESS, whilst maintaining a high q-resolution due to the long flight path. The q-range coverage is up to 20 angstrom(-1) allowing low-resolution PDF analysis. With the addition of SANS, HEIMDAL will be able to cover a uniquely broad length scale within a single instrumental set-up. HEIMDAL will be able to accommodate modern materials research in a broad variety of fields, and the task of the instrument will be to study advanced functional materials in action, as in situ and in operandi at multiple length scales (0.01-100 nm) quasi simultaneously. The instrument combines state-of-the-art neutron scattering techniques (TNPD, SANS, and NI) with the goal of studying real materials, in real time, under real conditions. This article describes the instrument design ideas, calculations and results of simulations and virtual experiments. (C) 2016 Elsevier B.V. All rights reserved.
引用
收藏
页码:229 / 241
页数:13
相关论文
共 25 条
[1]  
Andersen K., 2015, COMMUNICATION
[2]  
[Anonymous], 2015, INTERNAL REPORT NEW
[3]   A combined SAXS/WAXS/XAFS setup capable of observing concurrent changes across the nano-to-micrometer size range in inorganic solid crystallization processes [J].
Beale, Andrew M. ;
van der Eerden, Ad M. J. ;
Jacques, Simon D. M. ;
Leynaud, Olivier ;
O'Brien, Matthew G. ;
Meneau, Florian ;
Nikitenko, Sergei ;
Bras, Wim ;
Weckhuysen, Bert M. .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2006, 128 (38) :12386-12387
[4]  
Bertelsen M., 2014, THESIS U COPENHAGEN
[5]   NIMROD: The Near and InterMediate Range Order Diffractometer of the ISIS second target station [J].
Bowron, D. T. ;
Soper, A. K. ;
Jones, K. ;
Ansell, S. ;
Birch, S. ;
Norris, J. ;
Perrott, L. ;
Riedel, D. ;
Rhodes, N. J. ;
Wakefield, S. R. ;
Botti, A. ;
Ricci, M. -A. ;
Grazzi, F. ;
Zoppi, M. .
REVIEW OF SCIENTIFIC INSTRUMENTS, 2010, 81 (03)
[6]   Applications of principal component analysis to pair distribution function data [J].
Chapman, Karena W. ;
Lapidus, Saul H. ;
Chupas, Peter J. .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2015, 48 :1619-1626
[7]  
Chapon L. C., 2011, Neutron News, V22, P22, DOI [DOI 10.1080/10448632.2011.569650, 10.1080/10448632.2011.569650]
[8]   D33 - a third small-angle neutron scattering instrument at the Institut Laue Langevin [J].
Dewhurst, C. D. .
MEASUREMENT SCIENCE AND TECHNOLOGY, 2008, 19 (03)
[9]   iFit: A new data analysis framework. Applications for data reduction and optimization of neutron scattering instrument simulations with McStas [J].
Farhi, E. ;
Debab, Y. ;
Willendrup, P. .
JOURNAL OF NEUTRON RESEARCH, 2014, 17 (01) :5-18
[10]   In situ and real-time monitoring of mechanochemical milling reactions using synchrotron X-ray diffraction [J].
Halasz, Ivan ;
Kimber, Simon A. J. ;
Beldon, Patrick J. ;
Belenguer, Ana M. ;
Adams, Frank ;
Honkimaeki, Veijo ;
Nightingale, Richard C. ;
Dinnebier, Robert E. ;
Friscic, Tomislav .
NATURE PROTOCOLS, 2013, 8 (09) :1718-1729