Synthesis and characterization of cobalt-iron Prussian blue analogue nanoparticles by microemulsion

被引:0
|
作者
Fang Jian
Du Xian-Long
Lu Hui-Hong
Guo Dan
Zhao Ji-Hua [1 ]
Shen We-Guo
机构
[1] Lanzhou Univ, Dept Chem, Lanzhou 730000, Peoples R China
[2] E China Univ Sci & Technol, Dept Chem, Shanghai 200237, Peoples R China
关键词
microemulsion; triton X-100; Prussian blue analogues; nanoparticle;
D O I
暂无
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
Highly oriented cubic, hollow cubic and spherical nanoparticles of cobalt-iron Prussian blue analogues were synthesized in poly oxyethylene tertoctylphenyl ether (TritonX-100)/n-hexanol/cyclohexane microemulsion. The effects of the water-to-surfactant molar ratio (w), the reactant concentration and the reaction temperature on the morphology of cobalt-iron Prussian blue analogues were studied. The samples were characterized by transmission electron microscopy (TEM), field emission scan electron microscopy (FE-SEM), energy-dispersive X-ray spectroscopy (EDS), X-ray diffraction (XRD) and infrared spectroscopy (IR).
引用
收藏
页码:923 / 927
页数:5
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