1,1′-(Ethane-1,2-diyl)bis(1,4,7-triazonane)

被引：1

作者：

Knight, James C. ^{[1
]}

Fallis, Ian A. ^{[1
]}

机构：

[1] Cardiff Univ, Sch Chem, Cardiff CF10 3AT, S Glam, Wales

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷

基金：

英国工程与自然科学研究理事会;

关键词：

PHOTOSYSTEM-II; COMPLEXES; MODELS;

D O I：

10.1107/S1600536810019562

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the centrosymmetric title compound (dtne), C(14)H(32)N(6), two 1,4,7-triazacyclononane (tacn, or 1,4,7-triazonane) moieties are linked together each at an amino position by a single ethylene spacer. The molecular packing is supported by pairs of intermolecular N-H center dot center dot center dot N hydrogen bonds, which form R(2)(2)(22) ring motifs and link the molecules into infinite chains running parallel to the a axis.

引用

页码：O1513 / U2308

页数：10

共 13 条

[1] COMPLETION AND REFINEMENT OF CRYSTAL-STRUCTURES WITH SIR92 [J].

ALTOMARE, A ;

CASCARANO, G ;

GIACOVAZZO, C ;

GUAGLIARDI, A .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1993, 26 (pt 3) :343-350

[2]

Barbour L.J., 2001, J SUPRAMOL CHEM, V1, P189, DOI [DOI 10.1016/S1472-7862(02)00030-8, 10.1016/S1472-7862(02)00030-8]

[3] 1,4,7-Triazacyclononane hemihydrate [J].

Battle, AR ;

Johnson, DL ;

Martin, LL .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 :O330-O332

[4] PATTERNS IN HYDROGEN BONDING - FUNCTIONALITY AND GRAPH SET ANALYSIS IN CRYSTALS [J].

BERNSTEIN, J ;

DAVIS, RE ;

SHIMONI, L ;

CHANG, NL .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 1995, 34 (15) :1555-1573

[5] AN EMPIRICAL CORRECTION FOR ABSORPTION ANISOTROPY [J].

BLESSING, RH .

ACTA CRYSTALLOGRAPHICA SECTION A, 1995, 51 :33-38

[6] Synthesis and characterization of tris(bipyridyl)ruthenium(II)-modified mono-, di-, and trinuclear manganese complexes as electron-transfer models for photosystem II [J].

Burdinski, D ;

Bothe, E ;

Wieghardt, K .

INORGANIC CHEMISTRY, 2000, 39 (01) :105-116

[7] Crystal structure, superoxide dismutase activity and electrochemical property of complex [Cu(dtne)] • (ClO4)2 • CH3CH2OH [J].

Li, Qing-Xiang ;

Wang, Xiu-Feng ;

Cai, Li ;

Li, Qiao ;

Meng, Xiang-Gao ;

Xuan, Ai-Guo ;

Huang, Shao-Yun ;

Ai, Jun .

INORGANIC CHEMISTRY COMMUNICATIONS, 2009, 12 (02) :145-147

[8] Magnetic interactions in dinuclear MnIIIMnIV complexes covalently tethered to organic radicals:: Spectroscopic models for the S2YZ• state of photosystem II [J].

Marlin, DS ;

Bill, E ;

Weyhermüller, T ;

Bothe, E ;

Wieghardt, K .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2005, 127 (16) :6095-6108

[9]

Nonius, 2000, COLLECT

[10] Processing of X-ray diffraction data collected in oscillation mode [J].

Otwinowski, Z ;

Minor, W .

MACROMOLECULAR CRYSTALLOGRAPHY, PT A, 1997, 276 :307-326

← 1 2 →