Magnetic nanocatalyst;
Nanostructures;
Catalytic properties;
Chemical synthesis;
HIGHLY EFFICIENT SYNTHESIS;
ONE-POT SYNTHESIS;
MAGNETIC NANOPARTICLES;
HETEROGENEOUS CATALYST;
SUZUKI-MIYAURA;
IONIC LIQUID;
ACID;
NANOCATALYST;
DERIVATIVES;
FABRICATION;
D O I:
10.1016/j.solidstatesciences.2018.07.010
中图分类号:
O61 [无机化学];
学科分类号:
070301 ;
081704 ;
摘要:
In this paper all efforts have been devoted to develop stabilized tannic acid-SO3H on Fe3O4@SiO2 nanoparticles as the new magnetically and eco-friendly nanocatalyst. This nanocatalyst was identified using different techniques such as fourier transform infrared (FT-IR), Powder X-ray diffraction (XRD), vibrating sample magnetometry (VSM), scanning electron microscopy (SEM), energy dispersive x-ray spectroscopy (EDXS) and thermogravimetric analysis (TGA). Catalytic performance of the catalyst in cyclocondensation reaction of anthranilamide with different aldehydes under the friendly environmentally reaction condition led to formation corresponding 2,3-dihydro-4(1H)-quinazolinones compounds in excellent yields. The catalyst could be easily recovered by an external magnet and reused 4 times without significant loss of catalytic activity.
机构:
Univ Fed Rio Grande do Sul, Inst Chem, Av Bento Goncalves 9500, Porto Alegre, RS, BrazilUniv Fed Rio Grande do Sul, Inst Chem, Av Bento Goncalves 9500, Porto Alegre, RS, Brazil
Dido, Cezar A.
Mass, Eduardo B.
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Univ Fed Rio Grande do Sul, Inst Chem, Av Bento Goncalves 9500, Porto Alegre, RS, BrazilUniv Fed Rio Grande do Sul, Inst Chem, Av Bento Goncalves 9500, Porto Alegre, RS, Brazil
Mass, Eduardo B.
Pereira, Marcelo B.
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Univ Fed Rio Grande do Sul, Inst Phys, Av Bento Goncalves 9500, Porto Alegre, RS, BrazilUniv Fed Rio Grande do Sul, Inst Chem, Av Bento Goncalves 9500, Porto Alegre, RS, Brazil
Pereira, Marcelo B.
Hinrichs, Ruth
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Univ Fed Rio Grande do Sul, Inst Geosci, Av Bento Goncalves 9500, Porto Alegre, RS, BrazilUniv Fed Rio Grande do Sul, Inst Chem, Av Bento Goncalves 9500, Porto Alegre, RS, Brazil
Hinrichs, Ruth
D'Oca, Marcelo G. M.
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机构:
Fundacao Univ Fed Rio Grande, Av Italia, Rio Grande, BrazilUniv Fed Rio Grande do Sul, Inst Chem, Av Bento Goncalves 9500, Porto Alegre, RS, Brazil
D'Oca, Marcelo G. M.
Costa, Tania M. H.
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Univ Fed Rio Grande do Sul, Inst Chem, Av Bento Goncalves 9500, Porto Alegre, RS, BrazilUniv Fed Rio Grande do Sul, Inst Chem, Av Bento Goncalves 9500, Porto Alegre, RS, Brazil
Costa, Tania M. H.
Russowsky, Dennis
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Univ Fed Rio Grande do Sul, Inst Chem, Av Bento Goncalves 9500, Porto Alegre, RS, BrazilUniv Fed Rio Grande do Sul, Inst Chem, Av Bento Goncalves 9500, Porto Alegre, RS, Brazil
Russowsky, Dennis
Benvenutti, Edilson, V
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Univ Fed Rio Grande do Sul, Inst Chem, Av Bento Goncalves 9500, Porto Alegre, RS, BrazilUniv Fed Rio Grande do Sul, Inst Chem, Av Bento Goncalves 9500, Porto Alegre, RS, Brazil